Technology Process of alpha-D-Lyxofuranoside,ethyl2,3-O-(1-methylethylidene)-(9CI)
There total 5 articles about alpha-D-Lyxofuranoside,ethyl2,3-O-(1-methylethylidene)-(9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3 A molecular sieve; sodium cyanoborohydride; ethanolamine;
In
methanol;
at 20 ℃;
for 2h;
pH=6;
DOI:10.1016/S0008-6215(98)00313-9
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 88 percent / periodic acid / diethyl ether / 12 h / 20 °C
2: 66 percent / ethanolamine; 3A molecular sieves; sodium cyanoborohydride / methanol / 2 h / 20 °C / pH 6
With
3 A molecular sieve; sodium cyanoborohydride; ethanolamine; periodic acid;
In
methanol; diethyl ether;
1: Oxidation / 2: Reduction;
DOI:10.1016/S0008-6215(98)00313-9
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 76 percent / silver(I) oxide / dimethylformamide / 24 h / 20 °C
2: 88 percent / periodic acid / diethyl ether / 12 h / 20 °C
3: 66 percent / ethanolamine; 3A molecular sieves; sodium cyanoborohydride / methanol / 2 h / 20 °C / pH 6
With
3 A molecular sieve; sodium cyanoborohydride; ethanolamine; periodic acid; silver(l) oxide;
In
methanol; diethyl ether; N,N-dimethyl-formamide;
1: Etherification / 2: Oxidation / 3: Reduction;
DOI:10.1016/S0008-6215(98)00313-9
