3-(3-tert-butoxycarbonylaminopropoxy)-5-hydroxybenzoic acid 2,5-dioxopyrrolidin-1-yl ester

Base Information

Chemical Name:3-(3-tert-butoxycarbonylaminopropoxy)-5-hydroxybenzoic acid 2,5-dioxopyrrolidin-1-yl ester
CAS No.:1449061-21-5
Molecular Formula:C₁₉H₂₄N₂O₈
Molecular Weight:408.408
Hs Code.:

Synonyms:3-(3-tert-butoxycarbonylaminopropoxy)-5-hydroxybenzoic acid 2,5-dioxopyrrolidin-1-yl ester

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Chemical Property of 3-(3-tert-butoxycarbonylaminopropoxy)-5-hydroxybenzoic acid 2,5-dioxopyrrolidin-1-yl ester

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Technology Process of 3-(3-tert-butoxycarbonylaminopropoxy)-5-hydroxybenzoic acid 2,5-dioxopyrrolidin-1-yl ester

There total 4 articles about 3-(3-tert-butoxycarbonylaminopropoxy)-5-hydroxybenzoic acid 2,5-dioxopyrrolidin-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 1449061-20-4
3-(3-tert-butoxycarbonylaminopropoxy)-5-hydroxybenzoic acid

: 1449061-21-5
3-(3-tert-butoxycarbonylaminopropoxy)-5-hydroxybenzoic acid 2,5-dioxopyrrolidin-1-yl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; for 1h; Cooling with ice;

Reference yield:

: 83948-53-2
3-bromopropylamine tert-butylcarbamate

: 1449061-21-5
3-(3-tert-butoxycarbonylaminopropoxy)-5-hydroxybenzoic acid 2,5-dioxopyrrolidin-1-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide; acetone / 75 °C

2: water; sodium hydroxide / 20 °C

3: dicyclohexyl-carbodiimide / tetrahydrofuran / 1 h / Cooling with ice

With water; potassium carbonate; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1449061-19-1
3-(3-tert-butoxycarbonylaminopropoxy)-5-hydroxybenzoic acid methyl ester

: 1449061-21-5
3-(3-tert-butoxycarbonylaminopropoxy)-5-hydroxybenzoic acid 2,5-dioxopyrrolidin-1-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium hydroxide / 20 °C

2: dicyclohexyl-carbodiimide / tetrahydrofuran / 1 h / Cooling with ice

With water; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran;