C₂₂H₂₉NO₉

Base Information

Chemical Name:C₂₂H₂₉NO₉
CAS No.:946428-50-8
Molecular Formula:C₂₂H₂₉NO₉
Molecular Weight:451.474
Hs Code.:

C<sub>22</sub>H<sub>29</sub>NO<sub>9</sub>

Synonyms:C₂₂H₂₉NO₉

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Chemical Property of C₂₂H₂₉NO₉

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Technology Process of C₂₂H₂₉NO₉

There total 4 articles about C₂₂H₂₉NO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 946428-44-0
4-(o-methoxyphenyl)dehydroproline

: 105-53-3
diethyl malonate

: 946428-50-8
C₂₂H₂₉NO₉

Guidance literature:: diethyl malonate; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃;

4-(o-methoxyphenyl)dehydroproline; In tetrahydrofuran; Further stages.;
DOI:10.1021/ol070980t

Reference yield:

: N-carbomethoxy-L-3-dehydroproline methyl ester

: 946428-50-8
C₂₂H₂₉NO₉

Guidance literature:: Multi-step reaction with 2 steps

1.1: aq. AcOH / Pd(OAc)2 / acetonitrile / 4 h / 60 °C

1.2: 65 percent / 2,4-lutidine; trifluoroacetic anhydride / toluene

2.1: NaH / tetrahydrofuran / 0 - 20 °C

2.2: 79 percent / tetrahydrofuran

With sodium hydride; acetic acid; palladium diacetate; In tetrahydrofuran; acetonitrile; 2.2: Michael reaction;
DOI:10.1021/ol070980t

Reference yield:

: 492-95-5
2-methoxyphenyldiazonium tetrafluoroborate

: 946428-50-8
C₂₂H₂₉NO₉

Guidance literature:: Multi-step reaction with 2 steps

1.1: aq. AcOH / Pd(OAc)2 / acetonitrile / 4 h / 60 °C

1.2: 65 percent / 2,4-lutidine; trifluoroacetic anhydride / toluene

2.1: NaH / tetrahydrofuran / 0 - 20 °C

2.2: 79 percent / tetrahydrofuran

With sodium hydride; acetic acid; palladium diacetate; In tetrahydrofuran; acetonitrile; 2.2: Michael reaction;
DOI:10.1021/ol070980t