3-[3-[3-(hydroxymethyl)-5-methylsalicyl]-5-tert-butylsalicyl]-2-hydroxy-5-methylbenzyl alcohol

Base Information

Chemical Name:3-[3-[3-(hydroxymethyl)-5-methylsalicyl]-5-tert-butylsalicyl]-2-hydroxy-5-methylbenzyl alcohol
CAS No.:273755-69-4
Molecular Formula:C₂₈H₃₄O₅
Molecular Weight:450.575
Hs Code.:

Synonyms:3-[3-[3-(hydroxymethyl)-5-methylsalicyl]-5-tert-butylsalicyl]-2-hydroxy-5-methylbenzyl alcohol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-[3-[3-(hydroxymethyl)-5-methylsalicyl]-5-tert-butylsalicyl]-2-hydroxy-5-methylbenzyl alcohol

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Technology Process of 3-[3-[3-(hydroxymethyl)-5-methylsalicyl]-5-tert-butylsalicyl]-2-hydroxy-5-methylbenzyl alcohol

There total 4 articles about 3-[3-[3-(hydroxymethyl)-5-methylsalicyl]-5-tert-butylsalicyl]-2-hydroxy-5-methylbenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 72109-62-7
2-<5-tert-butylsalicyl-3-(5-methylsalicyl)>-4-methylphenol

: 273755-69-4
3-[3-[3-(hydroxymethyl)-5-methylsalicyl]-5-tert-butylsalicyl]-2-hydroxy-5-methylbenzyl alcohol

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; water; at 60 ℃; for 20h;
DOI:10.1080/00397910008087137

Reference yield:

: 2203-14-7
4-tert-butyl-2,5-bis(hydroxymethyl)phenol

: 273755-69-4
3-[3-[3-(hydroxymethyl)-5-methylsalicyl]-5-tert-butylsalicyl]-2-hydroxy-5-methylbenzyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / p-toluenesulfonic acid / benzene / 2 h / Heating

2: 53 percent / 25 percent aq. KOH / dioxane / 20 h / 60 °C

With potassium hydroxide; toluene-4-sulfonic acid; In 1,4-dioxane; benzene; 1: Condensation / 2: Alkylation;
DOI:10.1002/jhet.5570370516

Reference yield:

: 106-44-5
p-cresol

: 273755-69-4
3-[3-[3-(hydroxymethyl)-5-methylsalicyl]-5-tert-butylsalicyl]-2-hydroxy-5-methylbenzyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / p-toluenesulfonic acid / benzene / 2 h / Heating

2: 53 percent / 25 percent aq. KOH / dioxane / 20 h / 60 °C

With potassium hydroxide; toluene-4-sulfonic acid; In 1,4-dioxane; benzene; 1: Condensation / 2: Alkylation;
DOI:10.1002/jhet.5570370516