ethyl 3β,4β-bis(3',4'-dimethoxyphenyl)-1α,2α-cyclobutanedicarboxylate

Base Information

• Chemical Name: ethyl 3β,4β-bis(3',4'-dimethoxyphenyl)-1α,2α-cyclobutanedicarboxylate
• CAS No.: 201858-52-8
• Molecular Formula: C₂₆H₃₂O₈
• Molecular Weight: 472.535
• Mol file: 201858-52-8.mol

Synonyms:ethyl 3β,4β-bis(3',4'-dimethoxyphenyl)-1α,2α-cyclobutanedicarboxylate

Chemical Property of ethyl 3β,4β-bis(3',4'-dimethoxyphenyl)-1α,2α-cyclobutanedicarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl 3β,4β-bis(3',4'-dimethoxyphenyl)-1α,2α-cyclobutanedicarboxylate

There total 2 articles about ethyl 3β,4β-bis(3',4'-dimethoxyphenyl)-1α,2α-cyclobutanedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

ethyl (E)-3,4-dimethoxycinnamate (20583-78-2,24393-65-5) → ethyl 3β,4β-bis(3',4'-dimethoxyphenyl)-1α,2α-cyclobutanedicarboxylate (201858-52-8)

Guidance literature:

for 6h; Irradiation;

DOI:10.1021/jm991004l

Reference yield:

ethanol (64-17-5) + 3β,4β-bis(3',4'-dimethoxyphenyl)-1α,2α-cyclobutanedicarboxylic acid (201858-53-9) → ethyl 3β,4β-bis(3',4'-dimethoxyphenyl)-1α,2α-cyclobutanedicarboxylate (201858-52-8)

Guidance literature:

With sulfuric acid;

DOI:10.1016/0960-894X(96)00007-8

Reference yield: 97.0%

ethyl 3β,4β-bis(3',4'-dimethoxyphenyl)-1α,2α-cyclobutanedicarboxylate (201858-52-8) → 3β,4β-bis(3',4'-dimethoxyphenyl)-1α,2α-cyclobutanedicarboxylic acid (201858-53-9)

Guidance literature:

With potassium hydroxide; ethanol; for 6h;

DOI:10.1021/jm991004l

upstream raw materials:

ethanol

3β,4β-bis(3',4'-dimethoxyphenyl)-1α,2α-cyclobutanedicarboxylic acid

ethyl (E)-3,4-dimethoxycinnamate

Downstream raw materials:

3β,4β-bis(3',4'-dimethoxyphenyl)-1α,2α-cyclobutanedicarboxylic acid

methyl 3β,4β-bis(3',4'-dimethoxyphenyl)-1α,2α-cyclobutanedicarboxylate

tetrakis(Boc-caracasandiamide)