cyclohexyl 3-O-tert-butoxycarbonyl-2,4,6-tri-O-benzyl-β-D-allopyranoside

Base Information

Chemical Name:cyclohexyl 3-O-tert-butoxycarbonyl-2,4,6-tri-O-benzyl-β-D-allopyranoside
CAS No.:1083236-89-8
Molecular Formula:C₃₈H₄₈O₈
Molecular Weight:632.794
Hs Code.:

Synonyms:cyclohexyl 3-O-tert-butoxycarbonyl-2,4,6-tri-O-benzyl-β-D-allopyranoside

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Chemical Property of cyclohexyl 3-O-tert-butoxycarbonyl-2,4,6-tri-O-benzyl-β-D-allopyranoside

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Technology Process of cyclohexyl 3-O-tert-butoxycarbonyl-2,4,6-tri-O-benzyl-β-D-allopyranoside

There total 1 articles about cyclohexyl 3-O-tert-butoxycarbonyl-2,4,6-tri-O-benzyl-β-D-allopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1083236-85-4
phenyl 3-O-tert-butoxycarbonyl-2,4,6-tri-O-benzyl-1-thio-β-D-allopyranoside

: 108-93-0
cyclohexanol

: 1083236-86-5
2,4,6-tri-O-benzyl-1,3-O-carbonyl-α-D-allose

: 1083236-89-8
cyclohexyl 3-O-tert-butoxycarbonyl-2,4,6-tri-O-benzyl-β-D-allopyranoside

: 1083236-87-6
cyclohexyl 3-O-tert-butoxycarbonyl-2,4,6-tri-O-benzyl-α-D-allopyranoside

Guidance literature:: phenyl 3-O-tert-butoxycarbonyl-2,4,6-tri-O-benzyl-1-thio-β-D-allopyranoside; With 1-(phenylsulfonyl)piperidine; 2,4,5-tri-tert-butylpyrimidine; In dichloromethane; at -60 ℃; for 0.166667h; Molecular sieve; Inert atmosphere;

With trifluoromethylsulfonic anhydride; In dichloromethane; Inert atmosphere; Cooling;

cyclohexanol; In dichloromethane; at -60 ℃; for 2h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/jo801630m