4-pyrimidin-5-yl)ethyl>-N-methylamino>benzoic acid

Base Information

Chemical Name:4-pyrimidin-5-yl)ethyl>-N-methylamino>benzoic acid
CAS No.:170799-56-1
Molecular Formula:C₁₇H₂₁N₅O₂
Molecular Weight:327.386
Hs Code.:

4-<N-<2-(2,4-diamino-6,7-dihydro-5H-cyclopenta<d>pyrimidin-5-yl)ethyl>-N-methylamino>benzoic acid

Synonyms:4-pyrimidin-5-yl)ethyl>-N-methylamino>benzoic acid

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Chemical Property of 4-pyrimidin-5-yl)ethyl>-N-methylamino>benzoic acid

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Technology Process of 4-pyrimidin-5-yl)ethyl>-N-methylamino>benzoic acid

There total 10 articles about 4-pyrimidin-5-yl)ethyl>-N-methylamino>benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 170799-62-9
ethyl 4-pyrimidin-5-yl)ethyl>-N-methylamino>benzoate

: 170799-56-1
4-pyrimidin-5-yl)ethyl>-N-methylamino>benzoic acid

Guidance literature:: With hydrogenchloride; In acetic acid;
DOI:10.1248/cpb.43.829

Reference yield:

: 94-09-7
p-aminoethylbenzoate

: 170799-56-1
4-pyrimidin-5-yl)ethyl>-N-methylamino>benzoic acid

Guidance literature:: Multi-step reaction with 10 steps

1: 87 percent / N,N-diisopropylethylamine / dimethylformamide / 24 h / 70 °C

2: 63 percent / NaHCO₃ / 1 h / 90 °C

3: 55 percent / 1N NaOH / ethanol

4: 95 percent / NaBH₄

5: Et₃N

6: 93 percent / NaI

7: Bu₃SnH, AIBN / benzene / Heating

8: iso-Pr₂EtN / methanol

9: 59 percent

10: 96 percent / 1N HCl / acetic acid

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydrogencarbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; In methanol; ethanol; acetic acid; N,N-dimethyl-formamide; benzene;
DOI:10.1248/cpb.43.829

Reference yield:

: 170799-72-1
ethyl 4-benzoate

: 170799-56-1
4-pyrimidin-5-yl)ethyl>-N-methylamino>benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: Bu₃SnH, AIBN / benzene / Heating

2: iso-Pr₂EtN / methanol

3: 59 percent

4: 96 percent / 1N HCl / acetic acid

With hydrogenchloride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; N-ethyl-N,N-diisopropylamine; In methanol; acetic acid; benzene;
DOI:10.1248/cpb.43.829