bis(dimethylamino)mesitylphosphine

Base Information

• Chemical Name: bis(dimethylamino)mesitylphosphine
• CAS No.: 116005-25-5
• Molecular Formula: C₁₃H₂₃N₂P
• Molecular Weight: 238.313

Synonyms:bis(dimethylamino)mesitylphosphine

Chemical Property of bis(dimethylamino)mesitylphosphine

Chemical Property:

Purity/Quality:

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Technology Process of bis(dimethylamino)mesitylphosphine

There total 1 articles about bis(dimethylamino)mesitylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(N,N-dimethylamino)chlorophosphine (3348-44-5) + 2,4,6-trimethylphenyl bromide (576-83-0) → bis(dimethylamino)mesitylphosphine (116005-25-5)

Guidance literature:

With diethyl ether; magnesium; Multistep reaction; 2) THF, -45 grad C, 0.5 h;

DOI:10.1039/P19870001399

Reference yield: 61.0%

bis(dimethylamino)mesitylphosphine (116005-25-5) → dichloro(mesityl)phosphane (6781-96-0)

Guidance literature:

With hydrogenchloride; In pentane; Ambient temperature;

DOI:10.1021/ja00229a027

Reference yield:

bis(dimethylamino)mesitylphosphine (116005-25-5) → dichloro(mesityl)phosphane (6781-96-0) + N,N-dimethylammonium chloride (506-59-2)

Guidance literature:

With hydrogenchloride; at 0 ℃; for 1h; Yield given;

DOI:10.1039/P19870001399

upstream raw materials:

bis(N,N-dimethylamino)chlorophosphine

2,4,6-trimethylphenyl bromide

Downstream raw materials:

2-mesityl-3-phenyl-5-tert-butyl-1,3,2λ⁵-oxazaphosphorinane

dichloro(mesityl)phosphane

N,N-dimethylammonium chloride

MesP(O)Cl₂

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