Ph₂P(BH₃)CH₂CH(OH)C₆H₄NO₂-p

Base Information

Chemical Name:Ph₂P(BH₃)CH₂CH(OH)C₆H₄NO₂-p
CAS No.:97764-48-2
Molecular Formula:C₂₀H₂₁BNO₃P
Molecular Weight:365.176
Hs Code.:

Ph<sub>2</sub>P(BH<sub>3</sub>)CH<sub>2</sub>CH(OH)C<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>-p

Synonyms:Ph₂P(BH₃)CH₂CH(OH)C₆H₄NO₂-p

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Chemical Property of Ph₂P(BH₃)CH₂CH(OH)C₆H₄NO₂-p

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Technology Process of Ph₂P(BH₃)CH₂CH(OH)C₆H₄NO₂-p

There total 4 articles about Ph₂P(BH₃)CH₂CH(OH)C₆H₄NO₂-p which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 555-16-8
4-nitrobenzaldehdye

: 54067-17-3
diphenylmethylphosphine-borane complex

: 97764-48-2
Ph₂P(BH₃)CH₂CH(OH)C₆H₄NO₂-p

Guidance literature:: With sec.-butyllithium; In tetrahydrofuran; pentane; argon atmosphere; addn. of sec-butyllithium in pentane to soln. of Ph2MePBH3 in THF (-78°C), standig (-78°C, 2 h), addn. of p-O2NC6H4CHO, stirring (0.5 h); treatment with aq. HCl, extn. (ether), drying of extracts (MgSO4), preparative TLC (silica gel);
DOI:10.1021/ja00169a036

Reference yield:

: 2129-89-7
diphenyl(methyl)phosphine oxide

: 97764-48-2
Ph₂P(BH₃)CH₂CH(OH)C₆H₄NO₂-p

Guidance literature:: Multi-step reaction with 2 steps

1: CeCl₃*7H₂O; LiAlH₄ / tetrahydrofuran

2: sec-BuLi / tetrahydrofuran

With CeCl₃*7H₂O; LiAlH₄; sec-BuLi; In tetrahydrofuran;
DOI:10.1021/ja00304a061

Reference yield:

: 41593-58-2
diphenylphosphineborane

: 97764-48-2
Ph₂P(BH₃)CH₂CH(OH)C₆H₄NO₂-p

Guidance literature:: Multi-step reaction with 2 steps

1: MeI; KOH / methanol

2: sec-BuLi / tetrahydrofuran

With MeI; KOH; sec-BuLi; In tetrahydrofuran; methanol;
DOI:10.1021/ja00304a061