c-4-methoxy-1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-r-1-yl acetate

Base Information

Chemical Name:c-4-methoxy-1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-r-1-yl acetate
CAS No.:1224950-00-8
Molecular Formula:C₂₆H₃₀N₂O₄
Molecular Weight:434.535
Hs Code.:

Synonyms:c-4-methoxy-1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-r-1-yl acetate

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Chemical Property of c-4-methoxy-1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-r-1-yl acetate

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Technology Process of c-4-methoxy-1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-r-1-yl acetate

There total 10 articles about c-4-methoxy-1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-r-1-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1224949-08-9
c-4-hydroxy-1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-r-1-yl acetate

: 74-88-4
methyl iodide

: 1224950-00-8
c-4-methoxy-1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-r-1-yl acetate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 9h; Cooling with ice;

Reference yield:

: 70097-74-4
8-ethynyl-1,4-dioxaspiro[4.5]decan-8-ol

: 1224950-00-8
c-4-methoxy-1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-r-1-yl acetate

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.92 h / -72 °C

1.2: 0.58 h / -72 °C

2.1: manganese(IV) oxide / dichloromethane / 15 h / 20 °C

3.1: triethylamine / ethanol / 0.5 h / 20 °C

3.2: 15 h / 20 °C

4.1: hydrogenchloride; water / tetrahydrofuran / 15 h / 20 °C

4.2: 0 °C

5.1: sodium tetrahydroborate; methanol / 2 h / 20 °C

6.1: dmap; pyridine / dichloromethane / 66 h / 20 °C

7.1: potassium carbonate; methanol / 4 h / 20 °C

8.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 9 h / 20 °C / Cooling with ice

With pyridine; hydrogenchloride; methanol; dmap; manganese(IV) oxide; sodium tetrahydroborate; n-butyllithium; water; sodium hydride; potassium carbonate; triethylamine; In tetrahydrofuran; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1224950-00-8
c-4-methoxy-1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-r-1-yl acetate

Guidance literature:: Multi-step reaction with 10 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -76 °C

1.2: 2 h / -74 °C

2.1: potassium carbonate; methanol / 2 h / 20 °C

3.1: n-butyllithium / hexane; tetrahydrofuran / 0.92 h / -72 °C

3.2: 0.58 h / -72 °C

4.1: manganese(IV) oxide / dichloromethane / 15 h / 20 °C

5.1: triethylamine / ethanol / 0.5 h / 20 °C

5.2: 15 h / 20 °C

6.1: hydrogenchloride; water / tetrahydrofuran / 15 h / 20 °C

6.2: 0 °C

7.1: sodium tetrahydroborate; methanol / 2 h / 20 °C

8.1: dmap; pyridine / dichloromethane / 66 h / 20 °C

9.1: potassium carbonate; methanol / 4 h / 20 °C

10.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 9 h / 20 °C / Cooling with ice

With pyridine; hydrogenchloride; methanol; dmap; manganese(IV) oxide; sodium tetrahydroborate; n-butyllithium; water; sodium hydride; potassium carbonate; triethylamine; In tetrahydrofuran; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; mineral oil;