(E/Z)-(+/-)-3-(4-methoxyphenyl)-4-(3-methoxyphenyl)-14-pentylsulfonyltetradec-2-ene

Base Information

Chemical Name:(E/Z)-(+/-)-3-(4-methoxyphenyl)-4-(3-methoxyphenyl)-14-pentylsulfonyltetradec-2-ene
CAS No.:752225-76-6
Molecular Formula:C₃₃H₅₀O₄S
Molecular Weight:542.824
Hs Code.:

Synonyms:(E/Z)-(+/-)-3-(4-methoxyphenyl)-4-(3-methoxyphenyl)-14-pentylsulfonyltetradec-2-ene

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Chemical Property of (E/Z)-(+/-)-3-(4-methoxyphenyl)-4-(3-methoxyphenyl)-14-pentylsulfonyltetradec-2-ene

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Technology Process of (E/Z)-(+/-)-3-(4-methoxyphenyl)-4-(3-methoxyphenyl)-14-pentylsulfonyltetradec-2-ene

There total 3 articles about (E/Z)-(+/-)-3-(4-methoxyphenyl)-4-(3-methoxyphenyl)-14-pentylsulfonyltetradec-2-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 74-96-4
ethyl bromide

: 752225-70-0
(+/-)-1-(4-methoxyphenyl)-2-(3-methoxyphenyl)-12-pentylsulfonyldodecan-1-one

: 752225-76-6
(E/Z)-(+/-)-3-(4-methoxyphenyl)-4-(3-methoxyphenyl)-14-pentylsulfonyltetradec-2-ene

Guidance literature:: ethyl bromide; With iodine; magnesium; In diethyl ether; for 1h; Heating;

(+/-)-1-(4-methoxyphenyl)-2-(3-methoxyphenyl)-12-pentylsulfonyldodecan-1-one; In diethyl ether; for 2h; Heating;
DOI:10.1002/ardp.200400904

Reference yield:

: 98540-26-2
1′-(3-methoxyphenyl)-2′-(4′′-methoxyphenyl)ethan-2′-one

: 752225-76-6
(E/Z)-(+/-)-3-(4-methoxyphenyl)-4-(3-methoxyphenyl)-14-pentylsulfonyltetradec-2-ene

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 0 °C

1.2: 80 percent / dimethylformamide / 2 h / 20 °C

2.1: Mg tunings; iodine / diethyl ether / 1 h / Heating

2.2: 73 percent / diethyl ether / 2 h / Heating

With iodine; sodium hydride; magnesium; In diethyl ether; N,N-dimethyl-formamide; 2.1: Grignard reaction;
DOI:10.1002/ardp.200400904

Reference yield:

: 177584-01-9
1-bromo-10-(pentylsulfonyl)decane

: 752225-76-6
(E/Z)-(+/-)-3-(4-methoxyphenyl)-4-(3-methoxyphenyl)-14-pentylsulfonyltetradec-2-ene

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 0 °C

1.2: 80 percent / dimethylformamide / 2 h / 20 °C

2.1: Mg tunings; iodine / diethyl ether / 1 h / Heating

2.2: 73 percent / diethyl ether / 2 h / Heating

With iodine; sodium hydride; magnesium; In diethyl ether; N,N-dimethyl-formamide; 2.1: Grignard reaction;
DOI:10.1002/ardp.200400904