C₂₉H₃₂N₂O₃

Base Information

• Chemical Name: C₂₉H₃₂N₂O₃
• CAS No.: 91444-08-5
• Molecular Formula: C₂₉H₃₂N₂O₃
• Molecular Weight: 456.585
• Mol file: 91444-08-5.mol

Synonyms:C₂₉H₃₂N₂O₃

Chemical Property of C₂₉H₃₂N₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₂₉H₃₂N₂O₃

There total 1 articles about C₂₉H₃₂N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

ethylene glycol (107-21-1) + 1-Benzyl-8-(benzylamino)-6,9-dimethyl-2,5-dioxo-1,2,3,4,5,6-hexahydro-1-benzazocine (88609-66-9) → C29H32N2O3 (91444-08-5)

Guidance literature:

With camphor-10-sulfonic acid; at 80 - 90 ℃;

DOI:10.1021/ja00330a072

Reference yield:

C29H32N2O3 (91444-08-5) → C22H26N2O3

Guidance literature:

With hydrogen; palladium on activated charcoal; In acetic acid; ethyl acetate; Yield given;

DOI:10.1021/ja00330a072

Reference yield:

C29H32N2O3 (91444-08-5) → C29H32N2O5S

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / Pd-C / acetic acid; ethyl acetate

2: 94 percent / pyridine

With pyridine; hydrogen; palladium on activated charcoal; In acetic acid; ethyl acetate;

DOI:10.1021/ja00330a072

upstream raw materials:

ethylene glycol

1-Benzyl-8-(benzylamino)-6,9-dimethyl-2,5-dioxo-1,2,3,4,5,6-hexahydro-1-benzazocine