Technology Process of C15H8(2)H5N3O2
There total 4 articles about C15H8(2)H5N3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1,3-bis-(diphenylphosphino)propane; potassium acetate; palladium diacetate;
In
N,N-dimethyl-formamide;
at 110 ℃;
for 12h;
regioselective reaction;
Inert atmosphere;
Sealed tube;
DOI:10.1021/ja2007438
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium nitrate; trifluoroacetic acid
3.1: hydrogenchloride / acetonitrile / 0.25 h / -10 - 20 °C
3.2: 0.5 h / Cooling
3.3: 0.5 h / -10 - 20 °C
4.1: 1,3-bis-(diphenylphosphino)propane; potassium acetate; palladium diacetate / N,N-dimethyl-formamide / 12 h / 110 °C / Inert atmosphere; Sealed tube
With
hydrogenchloride; 1,3-bis-(diphenylphosphino)propane; potassium acetate; palladium diacetate; potassium nitrate; trifluoroacetic acid;
In
N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja2007438
- Guidance literature:
-
Multi-step reaction with 3 steps
2.1: hydrogenchloride / acetonitrile / 0.25 h / -10 - 20 °C
2.2: 0.5 h / Cooling
2.3: 0.5 h / -10 - 20 °C
3.1: 1,3-bis-(diphenylphosphino)propane; potassium acetate; palladium diacetate / N,N-dimethyl-formamide / 12 h / 110 °C / Inert atmosphere; Sealed tube
With
hydrogenchloride; 1,3-bis-(diphenylphosphino)propane; potassium acetate; palladium diacetate;
In
N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja2007438
