(2S,3S)-N-tert-butoxycarbonyl-2-[α-(2-methylphenoxy)phenylmethyl]morpholine

Base Information

Chemical Name:(2S,3S)-N-tert-butoxycarbonyl-2-[α-(2-methylphenoxy)phenylmethyl]morpholine
CAS No.:1097104-02-3
Molecular Formula:C₂₃H₂₉NO₄
Molecular Weight:383.488
Hs Code.:

Synonyms:(2S,3S)-N-tert-butoxycarbonyl-2-[α-(2-methylphenoxy)phenylmethyl]morpholine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-N-tert-butoxycarbonyl-2-[α-(2-methylphenoxy)phenylmethyl]morpholine

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Technology Process of (2S,3S)-N-tert-butoxycarbonyl-2-[α-(2-methylphenoxy)phenylmethyl]morpholine

There total 1 articles about (2S,3S)-N-tert-butoxycarbonyl-2-[α-(2-methylphenoxy)phenylmethyl]morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 847805-32-7
(+)-(2S,3S)-2-[α-hydroxy(phenyl)methyl]morpholine-4-carboxylic acid tert-butyl ester

: 32913-59-0
(η⁶-1-fluoro-2-methylbenzene)tricarbonylchromium(0)

: 1097104-02-3
(2S,3S)-N-tert-butoxycarbonyl-2-[α-(2-methylphenoxy)phenylmethyl]morpholine

Guidance literature:: (+)-(2S,3S)-2-[α-hydroxy(phenyl)methyl]morpholine-4-carboxylic acid tert-butyl ester; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 1h; Inert atmosphere;

(η⁶-1-fluoro-2-methylbenzene)tricarbonylchromium(0); In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 2h; Inert atmosphere;

With iodine; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/jm800817h