ethyl [4-phenyl-5-(N-p-tolylamino)methyl-1,2,4-triazol-3-yl]thioglycolate

Base Information

Chemical Name:ethyl [4-phenyl-5-(N-p-tolylamino)methyl-1,2,4-triazol-3-yl]thioglycolate
CAS No.:482652-40-4
Molecular Formula:C₂₀H₂₂N₄O₂S
Molecular Weight:382.486
Hs Code.:

Synonyms:ethyl [4-phenyl-5-(N-p-tolylamino)methyl-1,2,4-triazol-3-yl]thioglycolate

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Chemical Property of ethyl [4-phenyl-5-(N-p-tolylamino)methyl-1,2,4-triazol-3-yl]thioglycolate

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Technology Process of ethyl [4-phenyl-5-(N-p-tolylamino)methyl-1,2,4-triazol-3-yl]thioglycolate

There total 4 articles about ethyl [4-phenyl-5-(N-p-tolylamino)methyl-1,2,4-triazol-3-yl]thioglycolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 105-39-5
chloroacetic acid ethyl ester

: 92516-06-8
5-mercapto-4-phenyl-3-(N-p-tolylamino)methyl-1,2,4-triazole

: 482652-40-4
ethyl [4-phenyl-5-(N-p-tolylamino)methyl-1,2,4-triazol-3-yl]thioglycolate

Guidance literature:: 5-mercapto-4-phenyl-3-(N-p-tolylamino)methyl-1,2,4-triazole; With sodium hydroxide; In ethanol; for 0.75h; Heating;

chloroacetic acid ethyl ester; In ethanol; for 4h; Heating;

Reference yield:

: 2350-99-4
2-[(4-methylphenyl)amino]acetohydrazide

: 482652-40-4
ethyl [4-phenyl-5-(N-p-tolylamino)methyl-1,2,4-triazol-3-yl]thioglycolate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 86 percent / ethanol / 1 h / Heating

2.1: 79 percent / aq. NaOH / 3 h / Heating

3.1: NaOH / ethanol / 0.75 h / Heating

3.2: 70 percent / ethanol / 4 h / Heating

With sodium hydroxide; In ethanol;

Reference yield:

: 103-72-0
phenyl isothiocyanate

: 482652-40-4
ethyl [4-phenyl-5-(N-p-tolylamino)methyl-1,2,4-triazol-3-yl]thioglycolate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 86 percent / ethanol / 1 h / Heating

2.1: 79 percent / aq. NaOH / 3 h / Heating

3.1: NaOH / ethanol / 0.75 h / Heating

3.2: 70 percent / ethanol / 4 h / Heating

With sodium hydroxide; In ethanol;