Technology Process of C28H35N5O2
There total 3 articles about C28H35N5O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) chloride; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
dichloromethane;
at 20 ℃;
for 20h;
Inert atmosphere;
Schlenk technique;
Sealed tube;
DOI:10.1039/c4gc00031e
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 24 h / 20 °C / Inert atmosphere
2: toluene-4-sulfonic acid / methanol / 24 h / Reflux
3: potassium carbonate / acetonitrile; toluene / 0 - 20 °C / Inert atmosphere
4: copper(l) chloride; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / dichloromethane / 20 h / 20 °C / Inert atmosphere; Schlenk technique; Sealed tube
With
potassium carbonate; toluene-4-sulfonic acid; copper(l) chloride; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
methanol; dichloromethane; toluene; acetonitrile;
DOI:10.1039/c4gc00031e
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / methanol / 24 h / Reflux
2: potassium carbonate / acetonitrile; toluene / 0 - 20 °C / Inert atmosphere
3: copper(l) chloride; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / dichloromethane / 20 h / 20 °C / Inert atmosphere; Schlenk technique; Sealed tube
With
potassium carbonate; toluene-4-sulfonic acid; copper(l) chloride; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
methanol; dichloromethane; toluene; acetonitrile;
DOI:10.1039/c4gc00031e