Benzyl 3-O-benzyl-2-desoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:Benzyl 3-O-benzyl-2-desoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside
CAS No.:156520-24-0
Molecular Formula:C₃₁H₃₁NO₇
Molecular Weight:529.59
Hs Code.:

Synonyms:Benzyl 3-O-benzyl-2-desoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside

Suppliers and Price of Benzyl 3-O-benzyl-2-desoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl 3-O-benzyl-2-desoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of Benzyl 3-O-benzyl-2-desoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside

There total 5 articles about Benzyl 3-O-benzyl-2-desoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 100-39-0
benzyl bromide

: 151266-88-5
Benzyl 2-desoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside

: 156520-24-0
Benzyl 3-O-benzyl-2-desoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 16h; Ambient temperature;

Reference yield:

: 10022-13-6
1,3,4,6-tetra-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranose

: 156520-24-0
Benzyl 3-O-benzyl-2-desoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / trimethylsilyl triflate / CH₂Cl₂ / 2 h / Ambient temperature

2: conc. aq. HCl / acetone / 2.5 h

3: camphorsulfonic acid / 2 h

4: 92 percent / 55percent NaH / dimethylformamide / 16 h / Ambient temperature

With hydrogenchloride; trimethylsilyl trifluoromethanesulfonate; camphor-10-sulfonic acid; sodium hydride; In dichloromethane; N,N-dimethyl-formamide; acetone;

Reference yield:

: 80035-32-1
benzyl 2-deoxy-2-phthalimido-β-D-glucopyranoside

: 156520-24-0
Benzyl 3-O-benzyl-2-desoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: camphorsulfonic acid / 2 h

2: 92 percent / 55percent NaH / dimethylformamide / 16 h / Ambient temperature

With camphor-10-sulfonic acid; sodium hydride; In N,N-dimethyl-formamide;