4-(1-benzimidazolylmethyl)-N-(4-methylphenylsulfonyl)-1H-pyrrole-3-carboxaldehyde

Base Information

Chemical Name:4-(1-benzimidazolylmethyl)-N-(4-methylphenylsulfonyl)-1H-pyrrole-3-carboxaldehyde
CAS No.:1549717-03-4
Molecular Formula:C₂₀H₁₇N₃O₃S
Molecular Weight:379.439
Hs Code.:

Synonyms:4-(1-benzimidazolylmethyl)-N-(4-methylphenylsulfonyl)-1H-pyrrole-3-carboxaldehyde

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Chemical Property of 4-(1-benzimidazolylmethyl)-N-(4-methylphenylsulfonyl)-1H-pyrrole-3-carboxaldehyde

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Technology Process of 4-(1-benzimidazolylmethyl)-N-(4-methylphenylsulfonyl)-1H-pyrrole-3-carboxaldehyde

There total 2 articles about 4-(1-benzimidazolylmethyl)-N-(4-methylphenylsulfonyl)-1H-pyrrole-3-carboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 67-56-1
methanol

: 1549714-96-6
1-[4-(phenylsulfanylmethyl)-1-(4-methylphenylsulfonyl)-pyrrol-3-ylmethyl]benzimidazole

: 1549717-03-4
4-(1-benzimidazolylmethyl)-N-(4-methylphenylsulfonyl)-1H-pyrrole-3-carboxaldehyde

: 4-(1-benzimidazolylmethyl)-N-(4-methylphenylsulfonyl)-1H-pyrrole-3-carboxaldehyde dimethyl acetal

Guidance literature:: With ammonium cerium (IV) nitrate; at 20 ℃; for 24h;
DOI:10.1016/j.tet.2013.12.049

Reference yield:

: 1380676-39-0
4-methyl-N-(2-propyn-1-yl)-N-[3-(phenylthio)-2-propyn-1-yl]benzenesulfonamide

: 1549717-03-4
4-(1-benzimidazolylmethyl)-N-(4-methylphenylsulfonyl)-1H-pyrrole-3-carboxaldehyde

: 4-(1-benzimidazolylmethyl)-N-(4-methylphenylsulfonyl)-1H-pyrrole-3-carboxaldehyde dimethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: bis(hexafluoroacetylacetonato)nickel(II) monohydrate; bis-triphenylphosphine-palladium(II) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene / dimethyl sulfoxide / 1 h / 20 °C

2: ammonium cerium (IV) nitrate / 24 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; ammonium cerium (IV) nitrate; bis(hexafluoroacetylacetonato)nickel(II) monohydrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dimethyl sulfoxide;
DOI:10.1016/j.tet.2013.12.049