(3-benzyl-phenyl)-[5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-methanol

Base Information

Chemical Name:(3-benzyl-phenyl)-[5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-methanol
CAS No.:1280733-16-5
Molecular Formula:C₂₄H₂₀BrNO₂
Molecular Weight:434.332
Hs Code.:

Synonyms:(3-benzyl-phenyl)-[5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-methanol

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Chemical Property of (3-benzyl-phenyl)-[5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-methanol

Chemical Property:

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Technology Process of (3-benzyl-phenyl)-[5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-methanol

There total 5 articles about (3-benzyl-phenyl)-[5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1267684-96-7
5-(4-bromophenyl)-3-methylisoxazole-4-carbaldehyde

: 27798-39-6
1-benzyl-3-bromobenzene

: 1280733-16-5
(3-benzyl-phenyl)-[5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-methanol

Guidance literature:: 1-benzyl-3-bromobenzene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.25h;

5-(4-bromo-phenyl)-3-methyl-isoxazole-4-carbaldehyde; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

Reference yield:

: 85963-90-2
methyl 2-(4-bromobenzoyl)-3-oxo-butanoate

: 1280733-16-5
(3-benzyl-phenyl)-[5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-methanol

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydroxylamine hydrochloride; acetic acid / 1 h / 115 °C

2.1: lithium borohydride; ethanol / 60 °C

3.1: 4-methylmorpholine N-oxide / tetrapropylammonium perruthennate / dichloromethane

4.1: n-butyllithium / tetrahydrofuran / 0.25 h / -78 °C

4.2: 1 h / 0 - 20 °C

With lithium borohydride; n-butyllithium; ethanol; hydroxylamine hydrochloride; acetic acid; 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate; In tetrahydrofuran; dichloromethane;

Reference yield:

: 1228689-61-9
methyl 5-(4-bromophenyl)-3-methylisoxazole-4-carboxylate

: 1280733-16-5
(3-benzyl-phenyl)-[5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-methanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium borohydride; ethanol / 60 °C

2.1: 4-methylmorpholine N-oxide / tetrapropylammonium perruthennate / dichloromethane

3.1: n-butyllithium / tetrahydrofuran / 0.25 h / -78 °C

3.2: 1 h / 0 - 20 °C

With lithium borohydride; n-butyllithium; ethanol; 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate; In tetrahydrofuran; dichloromethane;