acetate d'hydroxymethyl-1 methoxy-4 dimethyl-3,3 cyclohexene-1

Base Information

• Chemical Name: acetate d'hydroxymethyl-1 methoxy-4 dimethyl-3,3 cyclohexene-1
• CAS No.: 73739-67-0
• Molecular Formula: C₁₂H₂₀O₃
• Molecular Weight: 212.289
• Mol file: 73739-67-0.mol

Synonyms:acetate d'hydroxymethyl-1 methoxy-4 dimethyl-3,3 cyclohexene-1

Chemical Property of acetate d'hydroxymethyl-1 methoxy-4 dimethyl-3,3 cyclohexene-1

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of acetate d'hydroxymethyl-1 methoxy-4 dimethyl-3,3 cyclohexene-1

There total 5 articles about acetate d'hydroxymethyl-1 methoxy-4 dimethyl-3,3 cyclohexene-1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

hydroxymethyl-1 methoxy-4 dimethyl-3,3 cyclohexene-1 (73739-63-6) + acetic anhydride (108-24-7) → acetate d'hydroxymethyl-1 methoxy-4 dimethyl-3,3 cyclohexene-1 (73739-67-0)

Guidance literature:

With pyridine; at 50 ℃; for 0.0833333h;

Reference yield:

2-methoxy-3,4-dihydro-2H-pyran (4454-05-1) → acetate d'hydroxymethyl-1 methoxy-4 dimethyl-3,3 cyclohexene-1 (73739-67-0)

Guidance literature:

Multi-step reaction with 5 steps

1: 55 percent / boron trifluoride-methanol complex / methanol / 4 h / Heating

2: 61 percent / boron trifluoride etherate / Ambient temperature

3: 95 percent / sodium acetate / acetic acid; H₂O / 4 h / Heating

4: 92 percent / NaBH₄ / methanol; H₂O / 1 h / Ambient temperature

5: 92 percent / pyridine / 0.08 h / 50 °C

With pyridine; sodium tetrahydroborate; boron trifluoride diethyl etherate; sodium acetate; boron trifluoride methanol complex; In methanol; water; acetic acid;

Reference yield:

1,1,5,5-tetramethoxy-pentane (4454-02-8) → acetate d'hydroxymethyl-1 methoxy-4 dimethyl-3,3 cyclohexene-1 (73739-67-0)

Guidance literature:

Multi-step reaction with 4 steps

1: 61 percent / boron trifluoride etherate / Ambient temperature

2: 95 percent / sodium acetate / acetic acid; H₂O / 4 h / Heating

3: 92 percent / NaBH₄ / methanol; H₂O / 1 h / Ambient temperature

4: 92 percent / pyridine / 0.08 h / 50 °C

With pyridine; sodium tetrahydroborate; boron trifluoride diethyl etherate; sodium acetate; In methanol; water; acetic acid;

upstream raw materials:

hydroxymethyl-1 methoxy-4 dimethyl-3,3 cyclohexene-1

acetic anhydride

2-methoxy-3,4-dihydro-2H-pyran

1,1,5,5-tetramethoxy-pentane

Downstream raw materials:

methoxy-5 methylene-2 dimethyl-6,6 cyclohexane acetate de dimethyltertiobutylsilyle

(3-Methoxy-2,2-dimethyl-6-methylene-cyclohexyl)-acetic acid methyl ester

(3-Methoxy-2,2-dimethyl-6-methylene-cyclohexyl)-acetyl chloride

acide methoxy-5 methylene-2 dimethyl-6,6 cyclohexane acetique