1L-(1,2,4/3,5)-1-C-(acetoxymethyl)-2,3,4,5-tetra-O-acetyl-1,2,3,4,5-cyclohexanepentol

Base Information

Chemical Name:1L-(1,2,4/3,5)-1-C-(acetoxymethyl)-2,3,4,5-tetra-O-acetyl-1,2,3,4,5-cyclohexanepentol
CAS No.:694527-29-2
Molecular Formula:C₁₇H₂₄O₁₁
Molecular Weight:404.371
Hs Code.:

Synonyms:1L-(1,2,4/3,5)-1-C-(acetoxymethyl)-2,3,4,5-tetra-O-acetyl-1,2,3,4,5-cyclohexanepentol

Suppliers and Price of 1L-(1,2,4/3,5)-1-C-(acetoxymethyl)-2,3,4,5-tetra-O-acetyl-1,2,3,4,5-cyclohexanepentol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1L-(1,2,4/3,5)-1-C-(acetoxymethyl)-2,3,4,5-tetra-O-acetyl-1,2,3,4,5-cyclohexanepentol

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 1L-(1,2,4/3,5)-1-C-(acetoxymethyl)-2,3,4,5-tetra-O-acetyl-1,2,3,4,5-cyclohexanepentol

There total 3 articles about 1L-(1,2,4/3,5)-1-C-(acetoxymethyl)-2,3,4,5-tetra-O-acetyl-1,2,3,4,5-cyclohexanepentol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108-24-7
acetic anhydride

: 115304-41-1
1L-(1,2,4/3,5)-1-C-(hydroxymethyl)-1,2,3,4,5-cyclohexanepentol

: 694527-29-2
1L-(1,2,4/3,5)-1-C-(acetoxymethyl)-2,3,4,5-tetra-O-acetyl-1,2,3,4,5-cyclohexanepentol

Guidance literature:: 1L-(1,2,4/3,5)-1-C-(hydroxymethyl)-1,2,3,4,5-cyclohexanepentol; With sodium acetate; In N,N-dimethyl-formamide; at 80 ℃; for 3h;

acetic anhydride; With pyridine; at 20 ℃; for 13h; Further stages.;
DOI:10.1039/b314795a

Reference yield:

: 693245-36-2
(3S,4S,5R,6S,7R)-4,5,6,7-tetrahydroxy-1-oxaspiro[2,5]octane

: 694527-29-2
1L-(1,2,4/3,5)-1-C-(acetoxymethyl)-2,3,4,5-tetra-O-acetyl-1,2,3,4,5-cyclohexanepentol

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / HBr / 50 °C

2: Zn; acetic acid / 2 h / Heating

With hydrogen bromide; acetic acid; zinc;
DOI:10.1081/CAR-200064653