C₂₁H₂₃N₅O₂*CH₂O₂

Base Information

Chemical Name:C₂₁H₂₃N₅O₂*CH₂O₂
CAS No.:1418002-28-4
Molecular Formula:CH₂O₂*C₂₁H₂₃N₅O₂
Molecular Weight:423.472
Hs Code.:

C<sub>21</sub>H<sub>23</sub>N<sub>5</sub>O<sub>2</sub>*CH<sub>2</sub>O<sub>2</sub>

Synonyms:C₂₁H₂₃N₅O₂*CH₂O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₂₃N₅O₂*CH₂O₂

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Technology Process of C₂₁H₂₃N₅O₂*CH₂O₂

There total 8 articles about C₂₁H₂₃N₅O₂*CH₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 64-18-6
formic acid

: 1418002-26-2
C₁₉H₂₁N₅

: 79-22-1
methyl chloroformate

: 1418002-28-4
C₂₁H₂₃N₅O₂*CH₂O₂

Guidance literature:: C₁₉H₂₁N₅; methyl chloroformate; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 ℃; for 1.5h;

formic acid;

Reference yield:

: 239074-29-4
trans (4-hydroxymethyl-cyclohexyl)-carbamic acid tert-butyl ester

: 1418002-28-4
C₂₁H₂₃N₅O₂*CH₂O₂

Guidance literature:: Multi-step reaction with 9 steps

1: pyridine / dichloromethane / 5 h / 0 - 20 °C

2: dimethyl sulfoxide / 4 h / 90 °C

3: trifluoroacetic acid / dichloromethane / 2.5 h / 20 °C

4: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 0.33 h / 120 °C / Microwave irradiation

5: ammonium chloride; iron / ethanol; water / 8.75 h / 80 °C

6: acetic acid / 0.5 h / 125 °C

7: sodium azide / N,N-dimethyl-formamide / 4 h / 20 °C

8: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; ethanol / 1.5 h / 20 °C / Inert atmosphere

9: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1.5 h / 0 °C

With pyridine; sodium azide; palladium 10% on activated carbon; hydrogen; iron; ammonium chloride; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 683269-95-6
N-[trans-4-[[(methylsulfonyl)oxy]methyl]cyclohexyl]carbamic acid tert-butyl ester

: 1418002-28-4
C₂₁H₂₃N₅O₂*CH₂O₂

Guidance literature:: Multi-step reaction with 8 steps

1: dimethyl sulfoxide / 4 h / 90 °C

2: trifluoroacetic acid / dichloromethane / 2.5 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 0.33 h / 120 °C / Microwave irradiation

4: ammonium chloride; iron / ethanol; water / 8.75 h / 80 °C

5: acetic acid / 0.5 h / 125 °C

6: sodium azide / N,N-dimethyl-formamide / 4 h / 20 °C

7: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; ethanol / 1.5 h / 20 °C / Inert atmosphere

8: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1.5 h / 0 °C

With sodium azide; palladium 10% on activated carbon; hydrogen; iron; ammonium chloride; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; isopropyl alcohol;