Z-4-nitro-N-(2,4-dinitrophenyl)-N-methylbenzenecarbohydrazonoyl chloride

Base Information

Chemical Name:Z-4-nitro-N-(2,4-dinitrophenyl)-N-methylbenzenecarbohydrazonoyl chloride
CAS No.:90913-84-1
Molecular Formula:C₁₄H₁₀ClN₅O₆
Molecular Weight:379.716
Hs Code.:

Synonyms:Z-4-nitro-N-(2,4-dinitrophenyl)-N-methylbenzenecarbohydrazonoyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Z-4-nitro-N-(2,4-dinitrophenyl)-N-methylbenzenecarbohydrazonoyl chloride

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Technology Process of Z-4-nitro-N-(2,4-dinitrophenyl)-N-methylbenzenecarbohydrazonoyl chloride

There total 2 articles about Z-4-nitro-N-(2,4-dinitrophenyl)-N-methylbenzenecarbohydrazonoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 90913-80-7
N-Methyl-N-(2,4-dinitrophenyl)-4-nitrobenzohydrazide

: 90913-84-1
Z-4-nitro-N-(2,4-dinitrophenyl)-N-methylbenzenecarbohydrazonoyl chloride

Guidance literature:: With phosphorus pentachloride; at 120 ℃; for 1h;
DOI:10.1021/jo00191a008

Reference yield:

: 19255-35-7
1-methyl-1-(2,4-dinitrophenyl)hydrazine

: 90913-84-1
Z-4-nitro-N-(2,4-dinitrophenyl)-N-methylbenzenecarbohydrazonoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 2 h / Heating

2: 67 percent / PCl₅ / 1 h / 120 °C

With phosphorus pentachloride; In pyridine;
DOI:10.1021/jo00191a008