(Z)-1-mesityl-2-((4aS,9aR)-4,4a,9,9a-tetrahydroindeno[2,1-b][1,4]oxazin-3(2H)-ylidene)hydrazine hydrochloride

Base Information

Chemical Name:(Z)-1-mesityl-2-((4aS,9aR)-4,4a,9,9a-tetrahydroindeno[2,1-b][1,4]oxazin-3(2H)-ylidene)hydrazine hydrochloride
CAS No.:955378-07-1
Molecular Formula:C₂₀H₂₃N₃O*ClH
Molecular Weight:357.883
Hs Code.:

Synonyms:(Z)-1-mesityl-2-((4aS,9aR)-4,4a,9,9a-tetrahydroindeno[2,1-b][1,4]oxazin-3(2H)-ylidene)hydrazine hydrochloride

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Chemical Property of (Z)-1-mesityl-2-((4aS,9aR)-4,4a,9,9a-tetrahydroindeno[2,1-b][1,4]oxazin-3(2H)-ylidene)hydrazine hydrochloride

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Technology Process of (Z)-1-mesityl-2-((4aS,9aR)-4,4a,9,9a-tetrahydroindeno[2,1-b][1,4]oxazin-3(2H)-ylidene)hydrazine hydrochloride

There total 3 articles about (Z)-1-mesityl-2-((4aS,9aR)-4,4a,9,9a-tetrahydroindeno[2,1-b][1,4]oxazin-3(2H)-ylidene)hydrazine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: (4aR,9bR)-2-methoxy-4,4a,5,9b-tetrahydro-3H-indeno[1,2-6]pyridine

: 24006-09-5,76195-82-9
mesitylhydrazine hydrochloride

: 955378-07-1
(Z)-1-mesityl-2-((4aS,9aR)-4,4a,9,9a-tetrahydroindeno[2,1-b][1,4]oxazin-3(2H)-ylidene)hydrazine hydrochloride

Guidance literature:: (4aR,9bR)-2-methoxy-4,4a,5,9b-tetrahydro-3H-indeno[1,2-6]pyridine; mesitylhydrazine hydrochloride; In methanol; at 20 ℃;

With hydrogenchloride; In 1,4-dioxane; methanol; at 60 ℃; for 48h;

Reference yield:

: C₁₂H₁₃O₂N

: 24006-09-5,76195-82-9
mesitylhydrazine hydrochloride

: 955378-07-1
C₂₀H₂₃N₃O*ClH

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; methanol; at 60 ℃; for 2.5h; Inert atmosphere;
DOI:10.1021/ja302761d

Reference yield:

: 913718-34-0
(4aS,9aR)-4,4a,9,9a-tetrahydroindeno[2,1-b][1,4]oxazin-3(2H)-one

: 955378-07-1
C₂₀H₂₃N₃O*ClH

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 12 h / 23 °C / Inert atmosphere

2: hydrogenchloride / 1,4-dioxane; methanol / 2.5 h / 60 °C / Inert atmosphere

With hydrogenchloride; In 1,4-dioxane; methanol; dichloromethane;
DOI:10.1021/ja302761d