(+)-(5S,S(S))-(2E)-[4-(p-tolylsulfinyl)deca-1,3-dien-5-yloxy]triisobutylsilane

Base Information

Chemical Name:(+)-(5S,S(S))-(2E)-[4-(p-tolylsulfinyl)deca-1,3-dien-5-yloxy]triisobutylsilane
CAS No.:951133-52-1
Molecular Formula:C₂₉H₅₀O₂SSi
Molecular Weight:490.866
Hs Code.:

Synonyms:(+)-(5S,S(S))-(2E)-[4-(p-tolylsulfinyl)deca-1,3-dien-5-yloxy]triisobutylsilane

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Chemical Property of (+)-(5S,S(S))-(2E)-[4-(p-tolylsulfinyl)deca-1,3-dien-5-yloxy]triisobutylsilane

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Technology Process of (+)-(5S,S(S))-(2E)-[4-(p-tolylsulfinyl)deca-1,3-dien-5-yloxy]triisobutylsilane

There total 3 articles about (+)-(5S,S(S))-(2E)-[4-(p-tolylsulfinyl)deca-1,3-dien-5-yloxy]triisobutylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 951133-45-2
(+)-(5S,S(S))-(4E)-4-(p-tolylsulfinyl)deca-1,3-dien-5-ol

: 13154-25-1
triiso-butylchlorosilane

: 951133-52-1
(+)-(5S,S(S))-(2E)-[4-(p-tolylsulfinyl)deca-1,3-dien-5-yloxy]triisobutylsilane

Guidance literature:: With dmap; triethylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1016/j.tetlet.2007.07.058

Reference yield:

: 66-25-1
hexanal

: 951133-52-1
(+)-(5S,S(S))-(2E)-[4-(p-tolylsulfinyl)deca-1,3-dien-5-yloxy]triisobutylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: LDA

2: 63 percent / Et₃N; DMAP / dimethylformamide / 0 - 20 °C

With dmap; triethylamine; lithium diisopropyl amide; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.07.058

Reference yield:

: 951133-73-6
(R)-(1,3-Butadienyl)-p-tolyl-sulfoxid

: 951133-52-1
(+)-(5S,S(S))-(2E)-[4-(p-tolylsulfinyl)deca-1,3-dien-5-yloxy]triisobutylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: LDA

2: 63 percent / Et₃N; DMAP / dimethylformamide / 0 - 20 °C

With dmap; triethylamine; lithium diisopropyl amide; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.07.058