ethyl 2-benzoylmethyl-2-ethoxycarbonyl-4-methyl-5-phenylmethyl-5-hexenoate

Base Information

Chemical Name:ethyl 2-benzoylmethyl-2-ethoxycarbonyl-4-methyl-5-phenylmethyl-5-hexenoate
CAS No.:1225287-65-9
Molecular Formula:C₂₇H₃₂O₅
Molecular Weight:436.548
Hs Code.:

Synonyms:ethyl 2-benzoylmethyl-2-ethoxycarbonyl-4-methyl-5-phenylmethyl-5-hexenoate

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Chemical Property of ethyl 2-benzoylmethyl-2-ethoxycarbonyl-4-methyl-5-phenylmethyl-5-hexenoate

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Technology Process of ethyl 2-benzoylmethyl-2-ethoxycarbonyl-4-methyl-5-phenylmethyl-5-hexenoate

There total 1 articles about ethyl 2-benzoylmethyl-2-ethoxycarbonyl-4-methyl-5-phenylmethyl-5-hexenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 93638-77-8
3-methyl-4-methylene-cyclopentane-1,1-dicarboxylic acid diethyl ester

: 100-58-3
phenylmagnesium bromide

: 70-11-1
α-bromoacetophenone

: 1225287-65-9
ethyl 2-benzoylmethyl-2-ethoxycarbonyl-4-methyl-5-phenylmethyl-5-hexenoate

Guidance literature:: phenylmagnesium bromide; With zinc dibromide; In tetrahydrofuran;

3-methyl-4-methylene-cyclopentane-1,1-dicarboxylic acid diethyl ester; With dibromobis(triphenylphosphine)nickel(II); In tetrahydrofuran; toluene; at 20 - 60 ℃; Inert atmosphere;

α-bromoacetophenone; In tetrahydrofuran; toluene; at 90 ℃; for 10h;
DOI:10.1021/ol100599c