[4-(5-bromo-4'-methoxy-biphenyl-3-ylmethoxy)-2-methyl-phenoxy]-acetic acid methyl ester

Base Information

Chemical Name:[4-(5-bromo-4'-methoxy-biphenyl-3-ylmethoxy)-2-methyl-phenoxy]-acetic acid methyl ester
CAS No.:870289-01-3
Molecular Formula:C₂₄H₂₃BrO₅
Molecular Weight:471.348
Hs Code.:

Synonyms:[4-(5-bromo-4'-methoxy-biphenyl-3-ylmethoxy)-2-methyl-phenoxy]-acetic acid methyl ester

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Chemical Property of [4-(5-bromo-4'-methoxy-biphenyl-3-ylmethoxy)-2-methyl-phenoxy]-acetic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of [4-(5-bromo-4'-methoxy-biphenyl-3-ylmethoxy)-2-methyl-phenoxy]-acetic acid methyl ester

There total 5 articles about [4-(5-bromo-4'-methoxy-biphenyl-3-ylmethoxy)-2-methyl-phenoxy]-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 868835-06-7
[4-(3,5-dibromobenzyloxy)-2-methylphenoxy]acetic acid methyl ester

: 5720-07-0
4-methoxyphenylboronic acid

: 870289-01-3
[4-(5-bromo-4'-methoxy-biphenyl-3-ylmethoxy)-2-methyl-phenoxy]-acetic acid methyl ester

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; ethanol; water; at 170 ℃; for 0.1h; Microwave irradiation;

Reference yield:

: 876-02-8
4-hydroxy-3-methylphenyl methyl ketone

: 870289-01-3
[4-(5-bromo-4'-methoxy-biphenyl-3-ylmethoxy)-2-methyl-phenoxy]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: caesium carbonate / acetonitrile / 20 °C

2: toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 48 h / Heating / reflux

3: sodium methylate / methanol / 1 h / 20 °C

4: caesium carbonate / acetonitrile / 18 h

5: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; ethanol; water / 0.1 h / 170 °C / Microwave irradiation

With sodium methylate; potassium carbonate; caesium carbonate; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; methanol; ethanol; dichloromethane; water; acetonitrile;

Reference yield:

: 317319-10-1
methyl (4-hydroxy-2-methylphenoxy)acetate

: 870289-01-3
[4-(5-bromo-4'-methoxy-biphenyl-3-ylmethoxy)-2-methyl-phenoxy]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / acetonitrile / 18 h

2: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; ethanol; water / 0.1 h / 170 °C / Microwave irradiation

With potassium carbonate; caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; ethanol; water; acetonitrile;