(S(p))-2-(diphenylphosphino)-1-(N-benzylcarbamoyl)ferrocene

Base Information

Chemical Name:(S(p))-2-(diphenylphosphino)-1-(N-benzylcarbamoyl)ferrocene
CAS No.:952679-06-0
Molecular Formula:C₃₀H₂₆FeNOP
Molecular Weight:503.363
Hs Code.:

Synonyms:(S(p))-2-(diphenylphosphino)-1-(N-benzylcarbamoyl)ferrocene

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Chemical Property of (S(p))-2-(diphenylphosphino)-1-(N-benzylcarbamoyl)ferrocene

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Technology Process of (S(p))-2-(diphenylphosphino)-1-(N-benzylcarbamoyl)ferrocene

There total 1 articles about (S(p))-2-(diphenylphosphino)-1-(N-benzylcarbamoyl)ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 677722-99-5,847675-62-1,297176-74-0
(Sp)-ortho-(diphenylphosphanyl)ferrocenylcarboxylic acid

: 100-46-9
benzylamine

: 952679-06-0
(S(p))-2-(diphenylphosphino)-1-(N-benzylcarbamoyl)ferrocene

Guidance literature:: With 1-hydroxybenzotriazole; N-[3-(dimethylamino)propyl]-N'-ethylcarbodiimide; In dichloromethane; under Ar atm. with exclusion direct daylight suspn. HOBt and ferrocene carboxylic acid in CH2Cl2 was stirred at 0°C for 5 min, EDC was added slowly and stirred at 0°C for 30 min amine in CH2Cl2 was added and stirred at room temp. for 20 h; react. mixt. was extd. with 3 M HCl, aq. NaHCO3 soln. and brine, org. phase was separated, dried over MgSO4 and evapd. in vacuo, column chromy. on silica (CH2Cl2-MeOH 20:1);
DOI:10.1021/om700542s

Reference yield: 75.0%

: di-μ-chlorido-bis(η3-1,3-diphenylallyl)dipalladium(II)

: 75-09-2
dichloromethane

: 952679-06-0
(S(p))-2-(diphenylphosphino)-1-(N-benzylcarbamoyl)ferrocene

: silver perchlorate

: (η3-1,3-diphenylallyl)[(S(p))-2-(diphenylphosphino)-1-(N-benzylcarbamoyl)ferrocene-κ2O,P]palladium(II) perchlorate*1.8CH2Cl2

: silver(I) chloride

Guidance literature:: In dichloromethane; under Ar atm. with exclusion direct daylight suspn. Fe and Pd complexes in CH2Cl2 was stirred at room temp. for 15 min, AgClO4 was added and stirred for 1 h; soln. was filtered and layered with Et2O, kept at 4°C for severaldays, ppt. was isolated by suction and dried in vacuo;
DOI:10.1021/om700542s