2'-iodobenzyl 2,3-di-O-acetyl-4-O-triethylsilyl-1-thio-β-D-xylopyranoside

Base Information

Chemical Name:2'-iodobenzyl 2,3-di-O-acetyl-4-O-triethylsilyl-1-thio-β-D-xylopyranoside
CAS No.:162088-95-1
Molecular Formula:C₂₂H₃₃IO₆SSi
Molecular Weight:580.556
Hs Code.:

Synonyms:2'-iodobenzyl 2,3-di-O-acetyl-4-O-triethylsilyl-1-thio-β-D-xylopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-iodobenzyl 2,3-di-O-acetyl-4-O-triethylsilyl-1-thio-β-D-xylopyranoside

Chemical Property:

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Technology Process of 2'-iodobenzyl 2,3-di-O-acetyl-4-O-triethylsilyl-1-thio-β-D-xylopyranoside

There total 5 articles about 2'-iodobenzyl 2,3-di-O-acetyl-4-O-triethylsilyl-1-thio-β-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59473-45-9
2-(chloromethyl)iodobenzene

: 162088-95-1
2'-iodobenzyl 2,3-di-O-acetyl-4-O-triethylsilyl-1-thio-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / K₂CO₃ / acetone; H₂O / 1.5 h / Ambient temperature

2: 74 percent / NaOMe / methanol

3: 1.) dibutyltin oxide / 1.) benzene, toluene, reflux, overnight, 2.) benzene, toluene, RT, 2 d

4: pyridine

With pyridine; sodium methylate; di(n-butyl)tin oxide; potassium carbonate; In methanol; water; acetone;
DOI:10.1016/0008-6215(94)00214-2

Reference yield:

: 2,3,4-tri-O-acetyl-1-thio-D-xylopyranose

: 162088-95-1
2'-iodobenzyl 2,3-di-O-acetyl-4-O-triethylsilyl-1-thio-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / K₂CO₃ / acetone; H₂O / 1.5 h / Ambient temperature

2: 74 percent / NaOMe / methanol

3: 1.) dibutyltin oxide / 1.) benzene, toluene, reflux, overnight, 2.) benzene, toluene, RT, 2 d

4: pyridine

With pyridine; sodium methylate; di(n-butyl)tin oxide; potassium carbonate; In methanol; water; acetone;
DOI:10.1016/0008-6215(94)00214-2

Reference yield:

: 162088-93-9
2'-iodobenzyl 2,3,4-tri-O-acetyl-1-thio-β-D-xylopyranoside

: 162088-95-1
2'-iodobenzyl 2,3-di-O-acetyl-4-O-triethylsilyl-1-thio-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / NaOMe / methanol

2: 1.) dibutyltin oxide / 1.) benzene, toluene, reflux, overnight, 2.) benzene, toluene, RT, 2 d

3: pyridine

With pyridine; sodium methylate; di(n-butyl)tin oxide; In methanol;
DOI:10.1016/0008-6215(94)00214-2