zinc pyrocatecholate

Base Information

• Chemical Name: zinc pyrocatecholate
• CAS No.: 10586-34-2
• Molecular Formula: C₆H₄O₂*Zn
• Molecular Weight: 173.487
• Mol file: 10586-34-2.mol

Synonyms:zinc pyrocatecholate

Chemical Property of zinc pyrocatecholate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of zinc pyrocatecholate

There total 3 articles about zinc pyrocatecholate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

diethylzinc (557-20-0) + benzene-1,2-diol (120-80-9,19481-10-8,37349-32-9) → ethane (74-84-0) + zinc pyrocatecholate (10586-34-2)

Guidance literature:

react. of the educts in a molar ratio of 1:1;

DOI:10.1016/0022-328X(90)87048-I

Reference yield: 82.0%

benzene-1,2-diol (120-80-9,19481-10-8,37349-32-9) + zinc (7440-66-6) → zinc pyrocatecholate (10586-34-2)

Guidance literature:

With Et₄NClO₄; In acetone; byproducts: H2; Electrochem. Process; under N2; oxidn. of the metal anode in a soln. containing NEt4ClO4 and the diol, initial voltage: 15 V (20 mA), 3 h; compd. is collected by filtn., washed with acetone and then diethylether, dried in vac., elem. anal.;

DOI:10.1016/S0020-1693(00)85905-8

Reference yield:

→ zinc pyrocatecholate (10586-34-2)

Guidance literature:

aus Brenzcatechin, Zn(II); Kinetik;

DOI:10.1021/ja01015a015

upstream raw materials:

benzene-1,2-diol

zinc

diethylzinc

Downstream raw materials:

ethane