2-(thien-2-ylmethylamino)-4-(N-methylanilino)-5-sulfamoylbenzene sulfonic acid phenyl ester

Base Information

Chemical Name:2-(thien-2-ylmethylamino)-4-(N-methylanilino)-5-sulfamoylbenzene sulfonic acid phenyl ester
CAS No.:80277-31-2
Molecular Formula:C₂₄H₂₃N₃O₅S₃
Molecular Weight:529.662
Hs Code.:

Synonyms:2-(thien-2-ylmethylamino)-4-(N-methylanilino)-5-sulfamoylbenzene sulfonic acid phenyl ester

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Chemical Property of 2-(thien-2-ylmethylamino)-4-(N-methylanilino)-5-sulfamoylbenzene sulfonic acid phenyl ester

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Technology Process of 2-(thien-2-ylmethylamino)-4-(N-methylanilino)-5-sulfamoylbenzene sulfonic acid phenyl ester

There total 4 articles about 2-(thien-2-ylmethylamino)-4-(N-methylanilino)-5-sulfamoylbenzene sulfonic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61791-73-9
4,6-dichlorobenzene-1,3-disulfonyl chloride

: 80277-31-2
2-(thien-2-ylmethylamino)-4-(N-methylanilino)-5-sulfamoylbenzene sulfonic acid phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NH₃ / 1.) THF, 5-10 deg C, 2 h, 2.) MeOH, a) reflux, 10 min, b) RT, overnight

2: 53 percent / 6 h / 140 °C

3: 2 h / 125 °C

With ammonia;
DOI:10.1021/jm00362a017

Reference yield:

: 108-95-2,27073-41-2
phenol

: 80277-31-2
2-(thien-2-ylmethylamino)-4-(N-methylanilino)-5-sulfamoylbenzene sulfonic acid phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NH₃ / 1.) THF, 5-10 deg C, 2 h, 2.) MeOH, a) reflux, 10 min, b) RT, overnight

2: 53 percent / 6 h / 140 °C

3: 2 h / 125 °C

With ammonia;
DOI:10.1021/jm00362a017