Technology Process of N,N-diallyl-4-methoxybenzamide
There total 1 articles about N,N-diallyl-4-methoxybenzamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; oxygen; copper(ll) bromide;
In
toluene;
at 110 ℃;
for 24h;
under 760.051 Torr;
Schlenk technique;
DOI:10.1055/s-0039-1690002
- Guidance literature:
-
With
(CH3)3SiCl; sodium; naphthalene;
In
tetrahydrofuran;
soln. of Na and C10H8 slowly added under Ar atm. to stirred suspn. of Fe(CO)5 at -78°C;warmed to 0°C;cooled to -78°C,(C3H5)2NC6H4(OCH3) soln. added,stirred for 30 min,then 30 min at 0°C;(CH3)3SiCl added,-78°C;stirred; solvent removed under reduced pressure on rotary evaporator; residue dried for several h under high vac.; hexane added; stirred vigorously for several min under Ar atm.; chromy.(alumina); eluted (hexane/CH2Cl2);
DOI:10.1016/j.electacta.2010.02.057
