N,N-diallyl-4-methoxybenzamide

Base Information

Chemical Name:N,N-diallyl-4-methoxybenzamide
CAS No.:39108-80-0
Molecular Formula:C₁₄H₁₇NO₂
Molecular Weight:231.294
Hs Code.:

Synonyms:N,N-diallyl-4-methoxybenzamide

Suppliers and Price of N,N-diallyl-4-methoxybenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N,N-diallyl-4-methoxybenzamide

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of N,N-diallyl-4-methoxybenzamide

There total 1 articles about N,N-diallyl-4-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 100-07-2
4-methoxy-benzoyl chloride

: 124-02-7
diallylamine

: 39108-80-0
N,N-diallyl-4-methoxybenzamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1055/s-0039-1690002

Reference yield: 93.0%

: 39108-80-0
N,N-diallyl-4-methoxybenzamide

: 70971-72-1
(4-methoxyphenyl)-(1H-pyrrol-1-yl)methanone

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; oxygen; copper(ll) bromide; In toluene; at 110 ℃; for 24h; under 760.051 Torr; Schlenk technique;
DOI:10.1055/s-0039-1690002

Reference yield: 26.0%

: 13463-40-6,71564-23-3,37220-42-1
iron pentacarbonyl

: 39108-80-0
N,N-diallyl-4-methoxybenzamide

: tricarbonyl[(η2-N-allyl-N-allylamino)(4-methoxyphenyl)methylene]iron(0)

Guidance literature:: With (CH₃)3SiCl; sodium; naphthalene; In tetrahydrofuran; soln. of Na and C10H8 slowly added under Ar atm. to stirred suspn. of Fe(CO)5 at -78°C;warmed to 0°C;cooled to -78°C,(C3H5)2NC6H4(OCH3) soln. added,stirred for 30 min,then 30 min at 0°C;(CH3)3SiCl added,-78°C;stirred; solvent removed under reduced pressure on rotary evaporator; residue dried for several h under high vac.; hexane added; stirred vigorously for several min under Ar atm.; chromy.(alumina); eluted (hexane/CH2Cl2);
DOI:10.1016/j.electacta.2010.02.057