3-(3,4,5-trimethoxyphenyl)propiolic acid 4-oxocyclohexyl ester

Base Information

Chemical Name:3-(3,4,5-trimethoxyphenyl)propiolic acid 4-oxocyclohexyl ester
CAS No.:1417611-61-0
Molecular Formula:C₁₈H₂₀O₆
Molecular Weight:332.353
Hs Code.:

Synonyms:3-(3,4,5-trimethoxyphenyl)propiolic acid 4-oxocyclohexyl ester

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Chemical Property of 3-(3,4,5-trimethoxyphenyl)propiolic acid 4-oxocyclohexyl ester

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Technology Process of 3-(3,4,5-trimethoxyphenyl)propiolic acid 4-oxocyclohexyl ester

There total 1 articles about 3-(3,4,5-trimethoxyphenyl)propiolic acid 4-oxocyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 4698-21-9
3-(3,4,5-trimethoxyphenyl)propiolic acid

: 13482-22-9
4-hydroxycyclohexanone

: 1417611-61-0
3-(3,4,5-trimethoxyphenyl)propiolic acid 4-oxocyclohexyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 49h;
DOI:10.1016/j.bmc.2012.11.019

Reference yield:

: 1417611-61-0
3-(3,4,5-trimethoxyphenyl)propiolic acid 4-oxocyclohexyl ester

: 27489-62-9
trans-4-hydroxycyclohexylamine

: 1417611-62-1
cis/trans-3-(3,4,5-trimethoxyphenyl)propiolic acid 4-(4-hydroxycyclohexylamino)cyclohexyl ester

: 1417611-63-2
trans/trans-3-(3,4,5-trimethoxyphenyl)propiolic acid 4-(4-hydroxycyclohexylamino)cyclohexyl ester

Guidance literature:: 3-(3,4,5-trimethoxyphenyl)propiolic acid 4-oxocyclohexyl ester; trans-4-hydroxycyclohexylamine; With titanium(IV) isopropylate; sodium cyanoborohydride; at 20 ℃; for 3h;

With sodium hydrogencarbonate; In ethanol; for 20h; Overall yield = 40 %; Overall yield = 370 mg;
DOI:10.1016/j.bmc.2012.11.019

Reference yield:

: 1417611-61-0
3-(3,4,5-trimethoxyphenyl)propiolic acid 4-oxocyclohexyl ester

: 6850-65-3,27489-62-9,40525-78-8
cis-4-aminocyclohexanol

: 1417611-64-3
cis/cis-3-(3,4,5-trimethoxyphenyl)propiolic acid 4-(4-hydroxycyclohexylamino)cyclohexyl ester

: 1417611-65-4
trans/cis-3-(3,4,5-trimethoxyphenyl)propiolic acid 4-(4-hydroxycyclohexylamino)cyclohexyl ester

Guidance literature:: 3-(3,4,5-trimethoxyphenyl)propiolic acid 4-oxocyclohexyl ester; cis-4-aminocyclohexanol; With titanium(IV) isopropylate; at 20 ℃; for 3h;

With sodium hydrogencarbonate; In ethanol; for 20h;
DOI:10.1016/j.bmc.2012.11.019