3-Ethyl-5,5-dimethyl-2-(triphenylphosphonioimino)-tetrahydro-3-furancarbonsaeure-ethylester-iodid

Base Information

Chemical Name:3-Ethyl-5,5-dimethyl-2-(triphenylphosphonioimino)-tetrahydro-3-furancarbonsaeure-ethylester-iodid
CAS No.:86300-10-9
Molecular Formula:C₂₉H₃₃NO₃P*I
Molecular Weight:601.464
Hs Code.:

Synonyms:3-Ethyl-5,5-dimethyl-2-(triphenylphosphonioimino)-tetrahydro-3-furancarbonsaeure-ethylester-iodid

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Chemical Property of 3-Ethyl-5,5-dimethyl-2-(triphenylphosphonioimino)-tetrahydro-3-furancarbonsaeure-ethylester-iodid

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Technology Process of 3-Ethyl-5,5-dimethyl-2-(triphenylphosphonioimino)-tetrahydro-3-furancarbonsaeure-ethylester-iodid

There total 3 articles about 3-Ethyl-5,5-dimethyl-2-(triphenylphosphonioimino)-tetrahydro-3-furancarbonsaeure-ethylester-iodid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 75-03-6
ethyl iodide

: 86299-98-1
4,5-Dihydro-5,5-dimethyl-2-(triphenylphosphoranylidenamino)-3-furancarbonsaeure-ethylester

: 86300-10-9
3-Ethyl-5,5-dimethyl-2-(triphenylphosphonioimino)-tetrahydro-3-furancarbonsaeure-ethylester-iodid

Guidance literature:: at 50 ℃; for 5h;

Reference yield:

: 2526-64-9
dichlorotriphenylphosphorane

: 86300-10-9
3-Ethyl-5,5-dimethyl-2-(triphenylphosphonioimino)-tetrahydro-3-furancarbonsaeure-ethylester-iodid

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / Et₃N, C₂Cl₆ / acetonitrile / 10 h / Ambient temperature

2: 75 percent / 5 h / 50 °C

With hexachloroethane; triethylamine; In acetonitrile;

Reference yield:

: 34859-61-5
ethyl 2-amino-5,5-dimethyl-4,5-dihydro-3-furancarboxylate

: 86300-10-9
3-Ethyl-5,5-dimethyl-2-(triphenylphosphonioimino)-tetrahydro-3-furancarbonsaeure-ethylester-iodid

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / Et₃N, C₂Cl₆ / acetonitrile / 10 h / Ambient temperature

2: 75 percent / 5 h / 50 °C

With hexachloroethane; triethylamine; In acetonitrile;