Technology Process of C8H5ClF8OS
There total 4 articles about C8H5ClF8OS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pentafluorosulfanyl chloride; dibenzoyl peroxide;
at 20 - 110 ℃;
for 8h;
Temperature;
Inert atmosphere;
DOI:10.1021/ol500766v
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium hydroxide; tetrabutylammomium bromide / 4 - 10 °C
2.1: potassium hydroxide / methanol / Inert atmosphere
2.2: 250 - 280 °C / Inert atmosphere
3.1: dibenzoyl peroxide; pentafluorosulfanyl chloride / 8 h / 20 - 110 °C / Inert atmosphere
With
pentafluorosulfanyl chloride; tetrabutylammomium bromide; potassium hydroxide; dibenzoyl peroxide;
In
methanol;
DOI:10.1021/ol500766v
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 100 °C / Autoclave; Inert atmosphere
2: 240 - 260 °C / Inert atmosphere; Pyrolysis
3: dibenzoyl peroxide; pentafluorosulfanyl chloride / 8 h / 20 - 110 °C / Inert atmosphere
With
pentafluorosulfanyl chloride; dibenzoyl peroxide;
DOI:10.1021/ol500766v