ethyl benzyloxymethyl<(diethoxyphosphoryl)methyl>phosphinate

Base Information

Chemical Name:ethyl benzyloxymethyl<(diethoxyphosphoryl)methyl>phosphinate
CAS No.:240432-41-1
Molecular Formula:C₁₅H₂₆O₆P₂
Molecular Weight:364.315
Hs Code.:

Synonyms:ethyl benzyloxymethyl<(diethoxyphosphoryl)methyl>phosphinate

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Chemical Property of ethyl benzyloxymethyl<(diethoxyphosphoryl)methyl>phosphinate

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Technology Process of ethyl benzyloxymethyl<(diethoxyphosphoryl)methyl>phosphinate

There total 3 articles about ethyl benzyloxymethyl<(diethoxyphosphoryl)methyl>phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 240432-39-7
ethyl hydrogen benzyloxymethylphosphonate

: 240432-41-1
ethyl benzyloxymethyl<(diethoxyphosphoryl)methyl>phosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride, DMF / benzene / 2.5 h / Ambient temperature

2: 1.) n-butyllithium / 1.) cyclohexane, THF, -78 deg C, 15 min, 2.) cyclohexane, THF, a) -78 deg C, 1 h, b) 0 deg C, 1 h

With n-butyllithium; oxalyl dichloride; N,N-dimethyl-formamide; In benzene;
DOI:10.1021/jm991008q

Reference yield:

: 89268-01-9
(phenylmethoxy)methylphosphonic acid diethyl ester

: 240432-41-1
ethyl benzyloxymethyl<(diethoxyphosphoryl)methyl>phosphinate

Guidance literature:: Multi-step reaction with 3 steps

1: 3.5 g / 1 M aq. KOH / ethanol / 2.5 h / 75 °C

2: oxalyl chloride, DMF / benzene / 2.5 h / Ambient temperature

3: 1.) n-butyllithium / 1.) cyclohexane, THF, -78 deg C, 15 min, 2.) cyclohexane, THF, a) -78 deg C, 1 h, b) 0 deg C, 1 h

With potassium hydroxide; n-butyllithium; oxalyl dichloride; N,N-dimethyl-formamide; In ethanol; benzene;
DOI:10.1021/jm991008q

Reference yield:

: 683-08-9
Diethyl methylphosphonate

: 240432-40-0
ethyl benzyloxymethyl(chloro)phosphonate

: 240432-41-1
ethyl benzyloxymethyl<(diethoxyphosphoryl)methyl>phosphinate

Guidance literature:: With n-butyllithium; Yield given; Multistep reaction; 1.) cyclohexane, THF, -78 deg C, 15 min, 2.) cyclohexane, THF, a) -78 deg C, 1 h, b) 0 deg C, 1 h;
DOI:10.1021/jm991008q