3-methoxy-2-nitroisonitrosoacetanilide

Base Information

Chemical Name:3-methoxy-2-nitroisonitrosoacetanilide
CAS No.:106987-80-8
Molecular Formula:C₉H₉N₃O₅
Molecular Weight:239.188
Hs Code.:

Synonyms:3-methoxy-2-nitroisonitrosoacetanilide

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Chemical Property of 3-methoxy-2-nitroisonitrosoacetanilide

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Technology Process of 3-methoxy-2-nitroisonitrosoacetanilide

There total 1 articles about 3-methoxy-2-nitroisonitrosoacetanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 302-17-0
chloral hydrate

: 16554-47-5
3-methoxy-2-nitroaniline

: 106987-80-8
3-methoxy-2-nitroisonitrosoacetanilide

Guidance literature:: With water; hydroxylamine sulfate; sodium sulfate; at 60 - 80 ℃; for 8h;
DOI:10.1021/jm00388a017

Reference yield:

: 106987-80-8
3-methoxy-2-nitroisonitrosoacetanilide

: 106976-20-9
2,3-diamino-4-methoxybenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / 80percent aq. H₂SO₄ / 0.25 h / 55 - 60 °C

2: 90 percent / 2N NaOH, 27percent aq. H₂O₂ / 0.25 h

3: H₂, NaOH / Pd/C / H₂O

With sodium hydroxide; sulfuric acid; hydrogen; dihydrogen peroxide; palladium on activated charcoal; In water;
DOI:10.1021/jm00388a017

Reference yield:

: 106987-80-8
3-methoxy-2-nitroisonitrosoacetanilide

: 106976-19-6
N-phenyl-3-amino-4-methoxyanthranilic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / 80percent aq. H₂SO₄ / 0.25 h / 55 - 60 °C

2: 90 percent / 2N NaOH, 27percent aq. H₂O₂ / 0.25 h

3: 1.) conc. H₂SO₄, NaNO₂, 85percent phosphoric acid, 2.) urea, 3.) KI

4: 50 percent / CuCl, Cu, N-ethylmorpholine / various solvent(s) / 15 h / 70 - 80 °C

5: NaBH₄, MeONa / methanol

With N-ethylmorpholine;; sodium hydroxide; sodium tetrahydroborate; phosphoric acid; sulfuric acid; dihydrogen peroxide; sodium methylate; copper; urea; potassium iodide; copper(l) chloride; sodium nitrite; In methanol;
DOI:10.1021/jm00388a017