N-tert-butoxycarbonyl-N'-(2-methoxyphenyl)-N'-(4-trifluoromethylphenyl)hydrazine

Base Information

Chemical Name:N-tert-butoxycarbonyl-N'-(2-methoxyphenyl)-N'-(4-trifluoromethylphenyl)hydrazine
CAS No.:1338369-69-9
Molecular Formula:C₁₉H₂₁F₃N₂O₃
Molecular Weight:382.383
Hs Code.:

Synonyms:N-tert-butoxycarbonyl-N'-(2-methoxyphenyl)-N'-(4-trifluoromethylphenyl)hydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-tert-butoxycarbonyl-N'-(2-methoxyphenyl)-N'-(4-trifluoromethylphenyl)hydrazine

Chemical Property:

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Technology Process of N-tert-butoxycarbonyl-N'-(2-methoxyphenyl)-N'-(4-trifluoromethylphenyl)hydrazine

There total 5 articles about N-tert-butoxycarbonyl-N'-(2-methoxyphenyl)-N'-(4-trifluoromethylphenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1338369-60-0
N-tert-butoxycarbonyl-N'-(4-trifluoromethylphenyl)diazene

: 100-66-3
methoxybenzene

: 1338369-69-9
N-tert-butoxycarbonyl-N'-(2-methoxyphenyl)-N'-(4-trifluoromethylphenyl)hydrazine

Guidance literature:: methoxybenzene; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

N-tert-butoxycarbonyl-N'-(4-trifluoromethylphenyl)diazene; In tetrahydrofuran; at -78 ℃; Inert atmosphere;
DOI:10.1055/s-0030-1260082

Reference yield:

: 937279-35-1
tert-butyl 2-(4-(trifluoromethyl)phenyl)hydrazine-1-carboxylate

: 1338369-69-9
N-tert-butoxycarbonyl-N'-(2-methoxyphenyl)-N'-(4-trifluoromethylphenyl)hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; N-Bromosuccinimide / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

With pyridine; N-Bromosuccinimide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-0030-1260082

Reference yield:

: 455-14-1
4-trifluoromethylphenylamine

: 1338369-69-9
N-tert-butoxycarbonyl-N'-(2-methoxyphenyl)-N'-(4-trifluoromethylphenyl)hydrazine

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride; sodium nitrite / water / 2.5 h / 0 °C / Inert atmosphere

2.1: hydrogenchloride; tin(II) chloride dihdyrate; water / 2.5 h / 0 °C / Inert atmosphere

3.1: tetrahydrofuran / 20 °C / Inert atmosphere

4.1: pyridine; N-Bromosuccinimide / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

5.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5.2: -78 °C / Inert atmosphere

With pyridine; hydrogenchloride; N-Bromosuccinimide; n-butyllithium; tin(II) chloride dihdyrate; N,N,N,N,-tetramethylethylenediamine; water; sodium nitrite; In tetrahydrofuran; dichloromethane; water;
DOI:10.1055/s-0030-1260082