tert-butyl 2-((cis-4-((methylsulfonyloxy)methyl)cyclohexyl)methoxy)acetate

Base Information

Chemical Name:tert-butyl 2-((cis-4-((methylsulfonyloxy)methyl)cyclohexyl)methoxy)acetate
CAS No.:1187856-35-4
Molecular Formula:C₁₅H₂₈O₆S
Molecular Weight:336.45
Hs Code.:

Synonyms:tert-butyl 2-((cis-4-((methylsulfonyloxy)methyl)cyclohexyl)methoxy)acetate

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Chemical Property of tert-butyl 2-((cis-4-((methylsulfonyloxy)methyl)cyclohexyl)methoxy)acetate

Chemical Property:

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Technology Process of tert-butyl 2-((cis-4-((methylsulfonyloxy)methyl)cyclohexyl)methoxy)acetate

There total 5 articles about tert-butyl 2-((cis-4-((methylsulfonyloxy)methyl)cyclohexyl)methoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1187856-34-3
tert-butyl 2-(((1s,4s)-4-(hydroxymethyl)cyclohexyl)methoxy)acetate

: 124-63-0
methanesulfonyl chloride

: 1187856-35-4
tert-butyl 2-((cis-4-((methylsulfonyloxy)methyl)cyclohexyl)methoxy)acetate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 5h;

Reference yield:

: 619-81-8
cis-cyclohexane-1,4-dicarboxylic acid

: 1187856-35-4
tert-butyl 2-((cis-4-((methylsulfonyloxy)methyl)cyclohexyl)methoxy)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

2: dirhodium tetraacetate / dichloromethane / 20 °C

3: triethylamine / dichloromethane / 5 h / 0 °C

With lithium aluminium tetrahydride; triethylamine; dirhodium tetraacetate; In tetrahydrofuran; dichloromethane;

Reference yield:

: 35059-50-8
t-butyl diazoacetate

: 1187856-35-4
tert-butyl 2-((cis-4-((methylsulfonyloxy)methyl)cyclohexyl)methoxy)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: dirhodium tetraacetate / dichloromethane / 20 °C

2: triethylamine / dichloromethane / 5 h / 0 °C

With triethylamine; dirhodium tetraacetate; In dichloromethane;