benzyl -α-diazoacetate

Base Information

Chemical Name:benzyl -α-diazoacetate
CAS No.:76530-01-3
Molecular Formula:C₂₂H₁₈N₂O₃
Molecular Weight:358.397
Hs Code.:

benzyl <p-(benzyloxy)phenyl>-α-diazoacetate

Synonyms:benzyl -α-diazoacetate

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Chemical Property of benzyl -α-diazoacetate

Chemical Property:

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Technology Process of benzyl -α-diazoacetate

There total 3 articles about benzyl -α-diazoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₂₆N₂O₅S

: 76530-01-3
benzyl -α-diazoacetate

Guidance literature:: With sodium; In ethylene glycol; at 70 ℃; Yield given;
DOI:10.1021/jo00321a007

Reference yield:

: 76529-99-2
benzyl glyoxylate

: 76530-01-3
benzyl -α-diazoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: Na / methanol / 1.) rom temp., 15 h 2.) 65 deg C, 1 h

2: Na / ethane-1,2-diol / 70 °C

With sodium; In methanol; ethylene glycol;
DOI:10.1021/jo00321a007

Reference yield:

: (4-Benzyloxy-phenyl)-hydroxy-acetic acid benzyl ester

: 76530-01-3
benzyl -α-diazoacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 22 percent / CrO₃ / pyridine / 5 h / Ambient temperature

2: Na / methanol / 1.) rom temp., 15 h 2.) 65 deg C, 1 h

3: Na / ethane-1,2-diol / 70 °C

With chromium(VI) oxide; sodium; In pyridine; methanol; ethylene glycol;
DOI:10.1021/jo00321a007