3,6-diaza-5-oxo-3-[2-((triphenylmethyl)thio)ethyl]-8-[(triphenylmethyl)thio]octanoic acid

Base Information

Chemical Name:3,6-diaza-5-oxo-3-[2-((triphenylmethyl)thio)ethyl]-8-[(triphenylmethyl)thio]octanoic acid
CAS No.:228253-42-7
Molecular Formula:C₄₆H₄₄N₂O₃S₂
Molecular Weight:736.999
Hs Code.:

Synonyms:3,6-diaza-5-oxo-3-[2-((triphenylmethyl)thio)ethyl]-8-[(triphenylmethyl)thio]octanoic acid

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Chemical Property of 3,6-diaza-5-oxo-3-[2-((triphenylmethyl)thio)ethyl]-8-[(triphenylmethyl)thio]octanoic acid

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Technology Process of 3,6-diaza-5-oxo-3-[2-((triphenylmethyl)thio)ethyl]-8-[(triphenylmethyl)thio]octanoic acid

There total 5 articles about 3,6-diaza-5-oxo-3-[2-((triphenylmethyl)thio)ethyl]-8-[(triphenylmethyl)thio]octanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: methyl 3,6-diaza-5-oxo-3-[2-((triphenylmethyl)thio)ethyl]-8-[(triphenylmethyl)thio]octanoate

: 228253-42-7
3,6-diaza-5-oxo-3-[2-((triphenylmethyl)thio)ethyl]-8-[(triphenylmethyl)thio]octanoic acid

Guidance literature:: methyl 3,6-diaza-5-oxo-3-[2-((triphenylmethyl)thio)ethyl]-8-[(triphenylmethyl)thio]octanoate; With potassium hydroxide; In methanol; at 20 ℃;

With hydrogenchloride; In methanol; water; pH=7;

Reference yield: 56.1%

: 79-08-3
bromoacetic acid

: 152863-83-7
N-[2-[(triphenylmethyl)thio]ethyl]-2-[[2-[(triphenylmethyl)thio]ethyl]amino]acetamide

: 228253-42-7
3,6-diaza-5-oxo-3-[2-((triphenylmethyl)thio)ethyl]-8-[(triphenylmethyl)thio]octanoic acid

Guidance literature:: With triethylamine; In acetonitrile; at 85 ℃;

Reference yield:

: 76-84-6
triphenylmethyl alcohol

: 228253-42-7
3,6-diaza-5-oxo-3-[2-((triphenylmethyl)thio)ethyl]-8-[(triphenylmethyl)thio]octanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / boron trifluoride diethyl etherate / chloroform / 4 h / 75 °C

2.1: triethylamine / chloroform / 2 h / 20 °C / Cooling with ice

3.1: triethylamine / dichloromethane / 48 h / Reflux

4.1: triethylamine / acetonitrile / 85 °C

5.1: potassium hydroxide / methanol / 20 °C

5.2: pH 7

With triethylamine; potassium hydroxide; boron trifluoride diethyl etherate; In methanol; dichloromethane; chloroform; acetonitrile;