1-(2,4-dinitrophenyl)-4-[(E)-2-(4-methoxyphenyl)vinyl]-3,5-dinitropyrazole

Base Information

Chemical Name:1-(2,4-dinitrophenyl)-4-[(E)-2-(4-methoxyphenyl)vinyl]-3,5-dinitropyrazole
CAS No.:1246929-39-4
Molecular Formula:C₁₈H₁₂N₆O₉
Molecular Weight:456.328
Hs Code.:

Synonyms:1-(2,4-dinitrophenyl)-4-[(E)-2-(4-methoxyphenyl)vinyl]-3,5-dinitropyrazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2,4-dinitrophenyl)-4-[(E)-2-(4-methoxyphenyl)vinyl]-3,5-dinitropyrazole

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Technology Process of 1-(2,4-dinitrophenyl)-4-[(E)-2-(4-methoxyphenyl)vinyl]-3,5-dinitropyrazole

There total 3 articles about 1-(2,4-dinitrophenyl)-4-[(E)-2-(4-methoxyphenyl)vinyl]-3,5-dinitropyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 123-11-5
4-methoxy-benzaldehyde

: 58333-00-9
1-(2,4-dinitrophenyl)-4-methyl-3,5-dinitropyrazole

: 1246929-39-4
1-(2,4-dinitrophenyl)-4-[(E)-2-(4-methoxyphenyl)vinyl]-3,5-dinitropyrazole

Guidance literature:: With morpholine; In xylenes; for 40h; Reflux;
DOI:10.1007/s11172-009-0288-8

Reference yield:

: 13808-75-8
1-(2,4-dinitrophenyl)-4-methylpyrazole

: 1246929-39-4
1-(2,4-dinitrophenyl)-4-[(E)-2-(4-methoxyphenyl)vinyl]-3,5-dinitropyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid; nitric acid / 3 h / 100 - 105 °C

2: morpholine / xylenes / 40 h / Reflux

With morpholine; sulfuric acid; nitric acid; In xylenes;
DOI:10.1007/s11172-009-0288-8

Reference yield:

: 119-26-6
(2,4-dinitro-phenyl)-hydrazine

: 1246929-39-4
1-(2,4-dinitrophenyl)-4-[(E)-2-(4-methoxyphenyl)vinyl]-3,5-dinitropyrazole

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / ethanol; water / 8 h / Reflux

2: sulfuric acid; nitric acid / 3 h / 100 - 105 °C

3: morpholine / xylenes / 40 h / Reflux

With morpholine; hydrogenchloride; sulfuric acid; nitric acid; In ethanol; water; xylenes;
DOI:10.1007/s11172-009-0288-8