N-(2-aminoethyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide

Base Information

Chemical Name:N-(2-aminoethyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide
CAS No.:1351184-57-0
Molecular Formula:C₂₀H₂₇N₃O₂S
Molecular Weight:373.519
Hs Code.:

Synonyms:N-(2-aminoethyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide

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Chemical Property of N-(2-aminoethyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide

Chemical Property:

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Technology Process of N-(2-aminoethyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide

There total 4 articles about N-(2-aminoethyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₂₉N₃O₄S

: 1351184-57-0
N-(2-aminoethyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide

Guidance literature:: C₂₈H₂₉N₃O₄S; With hydrazine; In ethanol; for 1h; Reflux;

With hydrogenchloride; In ethanol; water; for 4h; Reflux;
DOI:10.1016/j.bmc.2011.09.044

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 1351184-57-0
N-(2-aminoethyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / water / 0.5 h / 60 °C

2.1: tetrabutylammomium bromide; potassium carbonate; sodium hydroxide / toluene / 18 h / 60 °C / Reflux

3.1: hydrazine / ethanol / 1 h / Reflux

3.2: 4 h / Reflux

With tetrabutylammomium bromide; potassium carbonate; sodium hydroxide; hydrazine; In ethanol; water; toluene;
DOI:10.1016/j.bmc.2011.09.044

Reference yield:

: N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide

: 1351184-57-0
N-(2-aminoethyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrabutylammomium bromide; potassium carbonate; sodium hydroxide / toluene / 18 h / 60 °C / Reflux

2.1: hydrazine / ethanol / 1 h / Reflux

2.2: 4 h / Reflux

With tetrabutylammomium bromide; potassium carbonate; sodium hydroxide; hydrazine; In ethanol; toluene;
DOI:10.1016/j.bmc.2011.09.044