ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside
CAS No.:187152-77-8
Molecular Formula:C₂₉H₃₀O₆S
Molecular Weight:506.62
Hs Code.:

Synonyms:ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

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Chemical Property of ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

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Technology Process of ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

There total 4 articles about ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 98-88-4
benzoyl chloride

: 141810-60-8
ethyl 3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

: 187152-77-8
ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.tet.2010.08.004

Reference yield:

: 20701-61-5,56119-28-9,131564-36-8,142924-31-0,151123-92-1,141899-53-8
ethyl 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

: 187152-77-8
ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: di(n-butyl)tin oxide / methanol / 18 h / Inert atmosphere; Reflux

1.2: 24 h / 20 °C / Inert atmosphere

2.1: dmap / dichloromethane / 10 h / 20 °C / Cooling with ice

With dmap; di(n-butyl)tin oxide; In methanol; dichloromethane;
DOI:10.1039/d0ob00137f

Reference yield:

: 100-39-0
benzyl bromide

: 187152-77-8
ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: di(n-butyl)tin oxide / methanol / 18 h / Inert atmosphere; Reflux

1.2: 24 h / 20 °C / Inert atmosphere

2.1: dmap / dichloromethane / 10 h / 20 °C / Cooling with ice

With dmap; di(n-butyl)tin oxide; In methanol; dichloromethane;
DOI:10.1039/d0ob00137f