Technology Process of C23H20N2O5
There total 6 articles about C23H20N2O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate; water;
In
tetrahydrofuran;
at 20 - 25 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere
1.2: -78 - 25 °C
2.1: hydroxylamine hydrochloride; sodium acetate / methanol / 3 h / Reflux
3.1: pyridine; N-chloro-succinimide / tetrahydrofuran / 0.5 h / 55 °C
3.2: 0 - 5 °C
4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 25 °C
5.1: sodium tetrahydroborate; water / tetrahydrofuran / 2 h / 20 - 25 °C
With
pyridine; sodium tetrahydroborate; N-chloro-succinimide; hydroxylamine hydrochloride; water; sodium acetate; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; dichloromethane; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: Dess-Martin periodane / acetonitrile / 65 °C
2.1: hydroxylamine hydrochloride; sodium acetate / methanol / 3 h / Reflux
3.1: pyridine; N-chloro-succinimide / tetrahydrofuran / 0.5 h / 55 °C
3.2: 0 - 5 °C
4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 25 °C
5.1: sodium tetrahydroborate; water / tetrahydrofuran / 2 h / 20 - 25 °C
With
pyridine; sodium tetrahydroborate; N-chloro-succinimide; hydroxylamine hydrochloride; water; sodium acetate; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; dichloromethane; acetonitrile;
