2-(ω-bromoethylphenyl)-3-methoxyindenone

Base Information

Chemical Name:2-(ω-bromoethylphenyl)-3-methoxyindenone
CAS No.:136054-96-1
Molecular Formula:C₁₈H₁₅BrO₂
Molecular Weight:343.22
Hs Code.:

Synonyms:2-(ω-bromoethylphenyl)-3-methoxyindenone

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Chemical Property of 2-(ω-bromoethylphenyl)-3-methoxyindenone

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Technology Process of 2-(ω-bromoethylphenyl)-3-methoxyindenone

There total 10 articles about 2-(ω-bromoethylphenyl)-3-methoxyindenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 136054-95-0
Methanesulfonic acid 2-[2-(3-methoxy-1-oxo-1H-inden-2-yl)-phenyl]-ethyl ester

: 136054-96-1
2-(ω-bromoethylphenyl)-3-methoxyindenone

Guidance literature:: With lithium bromide; In tetrahydrofuran; for 0.75h; Heating;

Reference yield:

: 28272-96-0
2-vinylbenzaldehyde

: 136054-96-1
2-(ω-bromoethylphenyl)-3-methoxyindenone

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / sodium methoxide, ethyl propionate / methanol / 3 h / Heating

2: 98 percent / potassium carbonate / acetone / 1 h / Heating

3: 1.) 9-BBN, 2.) sodium acetate, hydrogen peroxide / 1.) THF, reflux, 5 h, 2.) RT, 2 h

4: 91 percent / triethylamine, dimethylaminopyridine / CH₂Cl₂ / 3 h / Ambient temperature

5: 90 percent / lithium bromide / tetrahydrofuran / 0.75 h / Heating

With dmap; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; sodium methylate; sodium acetate; potassium carbonate; Ethyl propionate; triethylamine; lithium bromide; In tetrahydrofuran; methanol; dichloromethane; acetone;

Reference yield:

: 4122-56-9
methyl o-formylbenzoate

: 136054-96-1
2-(ω-bromoethylphenyl)-3-methoxyindenone

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) sodamide / 1.) ether, RT, 4 h, 2.) RT, 15 min

2: 95 percent / diisobutylaluminium hydride (DBAL-H, 20percent in hexane) / CH₂Cl₂ / 0.5 h / -78 °C

3: 95 percent / manganese dioxide / CH₂Cl₂ / 3 h / Ambient temperature

4: 70 percent / sodium methoxide, ethyl propionate / methanol / 3 h / Heating

5: 98 percent / potassium carbonate / acetone / 1 h / Heating

6: 1.) 9-BBN, 2.) sodium acetate, hydrogen peroxide / 1.) THF, reflux, 5 h, 2.) RT, 2 h

7: 91 percent / triethylamine, dimethylaminopyridine / CH₂Cl₂ / 3 h / Ambient temperature

8: 90 percent / lithium bromide / tetrahydrofuran / 0.75 h / Heating

With dmap; manganese(IV) oxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; sodium methylate; sodium acetate; diisobutylaluminium hydride; potassium carbonate; sodium amide; Ethyl propionate; triethylamine; lithium bromide; In tetrahydrofuran; methanol; dichloromethane; acetone;