Methanesulfonic acid 2-[2-(3-methoxy-1-oxo-1H-inden-2-yl)-phenyl]-ethyl ester

Base Information

Chemical Name:Methanesulfonic acid 2-[2-(3-methoxy-1-oxo-1H-inden-2-yl)-phenyl]-ethyl ester
CAS No.:136054-95-0
Molecular Formula:C₁₉H₁₈O₅S
Molecular Weight:358.415
Hs Code.:

Synonyms:Methanesulfonic acid 2-[2-(3-methoxy-1-oxo-1H-inden-2-yl)-phenyl]-ethyl ester

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Chemical Property of Methanesulfonic acid 2-[2-(3-methoxy-1-oxo-1H-inden-2-yl)-phenyl]-ethyl ester

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Technology Process of Methanesulfonic acid 2-[2-(3-methoxy-1-oxo-1H-inden-2-yl)-phenyl]-ethyl ester

There total 9 articles about Methanesulfonic acid 2-[2-(3-methoxy-1-oxo-1H-inden-2-yl)-phenyl]-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 136054-94-9
2-(ω-hydroxyethylphenyl)-3-methoxyindenone

: 124-63-0
methanesulfonyl chloride

: 136054-95-0
Methanesulfonic acid 2-[2-(3-methoxy-1-oxo-1H-inden-2-yl)-phenyl]-ethyl ester

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 3h; Ambient temperature;

Reference yield:

: 28272-96-0
2-vinylbenzaldehyde

: 136054-95-0
Methanesulfonic acid 2-[2-(3-methoxy-1-oxo-1H-inden-2-yl)-phenyl]-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / sodium methoxide, ethyl propionate / methanol / 3 h / Heating

2: 98 percent / potassium carbonate / acetone / 1 h / Heating

3: 1.) 9-BBN, 2.) sodium acetate, hydrogen peroxide / 1.) THF, reflux, 5 h, 2.) RT, 2 h

4: 91 percent / triethylamine, dimethylaminopyridine / CH₂Cl₂ / 3 h / Ambient temperature

With dmap; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; sodium methylate; sodium acetate; potassium carbonate; Ethyl propionate; triethylamine; In methanol; dichloromethane; acetone;

Reference yield:

: 4122-56-9
methyl o-formylbenzoate

: 136054-95-0
Methanesulfonic acid 2-[2-(3-methoxy-1-oxo-1H-inden-2-yl)-phenyl]-ethyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) sodamide / 1.) ether, RT, 4 h, 2.) RT, 15 min

2: 95 percent / diisobutylaluminium hydride (DBAL-H, 20percent in hexane) / CH₂Cl₂ / 0.5 h / -78 °C

3: 95 percent / manganese dioxide / CH₂Cl₂ / 3 h / Ambient temperature

4: 70 percent / sodium methoxide, ethyl propionate / methanol / 3 h / Heating

5: 98 percent / potassium carbonate / acetone / 1 h / Heating

6: 1.) 9-BBN, 2.) sodium acetate, hydrogen peroxide / 1.) THF, reflux, 5 h, 2.) RT, 2 h

7: 91 percent / triethylamine, dimethylaminopyridine / CH₂Cl₂ / 3 h / Ambient temperature

With dmap; manganese(IV) oxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; sodium methylate; sodium acetate; diisobutylaluminium hydride; potassium carbonate; sodium amide; Ethyl propionate; triethylamine; In methanol; dichloromethane; acetone;