(E)-N-phenyl-N-(4-(2-(quinolin-2-yl)vinyl)phenyl)benzenamine

Base Information

• Chemical Name: (E)-N-phenyl-N-(4-(2-(quinolin-2-yl)vinyl)phenyl)benzenamine
• CAS No.: 1220212-19-0
• Molecular Formula: C₂₉H₂₂N₂
• Molecular Weight: 398.507
• Mol file: 1220212-19-0.mol

Synonyms:(E)-N-phenyl-N-(4-(2-(quinolin-2-yl)vinyl)phenyl)benzenamine

Chemical Property of (E)-N-phenyl-N-(4-(2-(quinolin-2-yl)vinyl)phenyl)benzenamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-N-phenyl-N-(4-(2-(quinolin-2-yl)vinyl)phenyl)benzenamine

There total 3 articles about (E)-N-phenyl-N-(4-(2-(quinolin-2-yl)vinyl)phenyl)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

2-methylquinoline (91-63-4) + [4-(diphenylamino)phenyl]methanol (25069-40-3) → (E)-N-phenyl-N-(4-(2-(quinolin-2-yl)vinyl)phenyl)benzenamine (1220212-19-0)

Guidance literature:

With potassium tert-butylate; nickel dibromide; N-(8-quinolyl)pyridine-2-carboxamide; In tert-butyl alcohol; at 140 ℃; for 48h; Schlenk technique; Inert atmosphere; Sealed tube;

DOI:10.1021/acs.joc.9b01517

Reference yield: 70.0%

2-methylquinoline (91-63-4) + 4-(diphenylamino)benzaldehyde (4181-05-9) → (E)-N-phenyl-N-(4-(2-(quinolin-2-yl)vinyl)phenyl)benzenamine (1220212-19-0)

Guidance literature:

2-methylquinoline; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.5h;

4-(diphenylamino)benzaldehyde; In tetrahydrofuran; at 0 ℃; for 2h;

DOI:10.1016/j.dyepig.2018.11.044

Reference yield: 58.0%

diphenylamine (122-39-4) → (E)-N-phenyl-N-(4-(2-(quinolin-2-yl)vinyl)phenyl)benzenamine (1220212-19-0)

Guidance literature:

With palladium diacetate; tris-(o-tolyl)phosphine; sodium t-butanolate; In toluene; at 110 ℃; Inert atmosphere;

DOI:10.3184/030823409X465286

upstream raw materials:

diphenylamine

2-methylquinoline

4-(diphenylamino)benzaldehyde

[4-(diphenylamino)phenyl]methanol