[((1,3-di-1-adamanthylimidazolin-2-ylidene)(+1H))][(hydride)B(pentafluorophenyl)3]

Base Information

Chemical Name:[((1,3-di-1-adamanthylimidazolin-2-ylidene)(+1H))][(hydride)B(pentafluorophenyl)3]
CAS No.:1313574-26-3
Molecular Formula:C₁₈HBF₁₅*C₂₃H₃₃N₂
Molecular Weight:850.521
Hs Code.:

Synonyms:[((1,3-di-1-adamanthylimidazolin-2-ylidene)(+1H))][(hydride)B(pentafluorophenyl)3]

Suppliers and Price of [((1,3-di-1-adamanthylimidazolin-2-ylidene)(+1H))][(hydride)B(pentafluorophenyl)3]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [((1,3-di-1-adamanthylimidazolin-2-ylidene)(+1H))][(hydride)B(pentafluorophenyl)3]

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Technology Process of [((1,3-di-1-adamanthylimidazolin-2-ylidene)(+1H))][(hydride)B(pentafluorophenyl)3]

There total 2 articles about [((1,3-di-1-adamanthylimidazolin-2-ylidene)(+1H))][(hydride)B(pentafluorophenyl)3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1109-15-5
tris(pentafluorophenyl)borate

: 131042-77-8
IAd

: 1313574-26-3
[((1,3-di-1-adamanthylimidazolin-2-ylidene)(+1H))][(hydride)B(pentafluorophenyl)3]

Guidance literature:: With hydrogen; In toluene; at -30 - 20 ℃; for 8.16667h;
DOI:10.1021/ic201290g

Reference yield: 89.0%

: 1109-15-5
tris(pentafluorophenyl)borate

: 1333-74-0
hydrogen

: 131042-77-8
IAd

: 1313574-26-3
[((1,3-di-1-adamanthylimidazolin-2-ylidene)(+1H))][(hydride)B(pentafluorophenyl)3]

Guidance literature:: In toluene; (Ar), Schlenk techniques; dissolving N compd., B compd. (1:1) in tolueneat -30°C under H2 atm., purging with H2 for 10 min, stirring und er H2 for 8 h at room temp.; evapn. in vacuo, stirring for 10 min with toluene/pentane (1:10), filtration, washing with pentane, drying in vacuo, elem. anal.;
DOI:10.1021/ic201290g