ethyl (1Z)-2-(3,4,5-trimethoxyphenyl)ethanimidoate

Base Information

• Chemical Name: ethyl (1Z)-2-(3,4,5-trimethoxyphenyl)ethanimidoate
• CAS No.: 93270-42-9
• Molecular Formula: C13H19 N O4 . Cl H
• Molecular Weight: 253.2943
• Mol file: 93270-42-9.mol

Synonyms:Benzeneethanimidicacid, 3,4,5-trimethoxy-, ethyl ester, hydrochloride (9CI)

Chemical Property of ethyl (1Z)-2-(3,4,5-trimethoxyphenyl)ethanimidoate

Chemical Property:

• Vapor Pressure: 0.000235mmHg at 25°C
• Boiling Point: 335.3°Cat760mmHg
• Flash Point: 156.6°C
• Density: 1.08g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl (1Z)-2-(3,4,5-trimethoxyphenyl)ethanimidoate

There total 2 articles about ethyl (1Z)-2-(3,4,5-trimethoxyphenyl)ethanimidoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

ethanol (64-17-5) + 2-(3,4,5-trimethoxyphenyl)acetonitrile (13338-63-1) → Ethyl 3,4,5-Trimethoxyphenylacetimidate Hydrochloride (93270-42-9)

Guidance literature:

With hydrogenchloride; Ambient temperature;

DOI:10.1002/jhet.5570260350

Reference yield:

2-(3,4,5-trimethoxyphenyl)acetonitrile (13338-63-1) → Ethyl 3,4,5-Trimethoxyphenylacetimidate Hydrochloride (93270-42-9)

Guidance literature:

Reference yield: 90.0%

Ethyl 3,4,5-Trimethoxyphenylacetimidate Hydrochloride (93270-42-9) + naphthalene-1,8-diamine (479-27-6) → 2-(3,4,5-trimethoxybenzyl)-1H-perimidine

Guidance literature:

In methanol; at 60 - 65 ℃; for 0.0833333h; Temperature; Time; Microwave irradiation;

DOI:10.3184/174751913X13691578103477

upstream raw materials:

2-(3,4,5-trimethoxyphenyl)acetonitrile

ethanol

Downstream raw materials:

2-(3,4,5-trimethoxy-benzyl)-4,5-dihydro-1H-imidazole

3,4,5-trimethoxyphenylmethyl-β-3,4,5-trimethoxyphenylacetylamidrazone

3-[2-(3,4,5-Trimethoxy-benzyl)-benzoimidazol-1-yl]-butyric acid

N-(2,2-Dimethoxy-ethyl)-2-(3,4,5-trimethoxy-phenyl)-acetamidine; hydrochloride